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North Coast Laboratories, Ltd Date 13-opt-05 <br /> CLIENT J L Analytical Services QC SUMMARY REPORT <br /> Work Order 0510087 <br /> Project 9-4235 Delta 76 Laboratory Control Spike <br /> Sample 1D LCS-05652 Batch ID R37390 Test Code 8260OXYW Units pg/L Analysis Date 10/11105 4 59 00 AM Prep Date <br /> Client ID Run ID ORGCMS3_051011B SegNci 538156 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Methyl tert butyl ether(MTBE) 1956 10 200 0 978% 80 120 0 <br /> Tert-butyl alcohol(TBA) 3992 10 400 0 998% 25 162 0 <br /> Di-isopropyl ether(RIPE) 1944 10 200 0 972% 80 120 0 <br /> Ethyl tert butyl ether(ETBE) 1918 10 200 0 959% 77 120 0 <br /> Benzene 20 03 0 50 200 0 100% 78 117 0 <br /> Tert amyl methyl ether(TAME) 1906 1 0 200 0 953% 64 136 0 <br /> Toluene 1997 0 50 200 0 998% 80 120 0 <br /> Ethylbenzene 1893 0 50 200 0 946% 80 120 0 <br /> m p-Xylene 38 96 050 400 0 974% 80 120 0 <br /> o-Xylene 1861 050 200 0 930% 80 120 0 <br /> 14-Dichlorobenzene-d4 109 010 100 0 109% 81 139 0 <br /> Sample ID LCSD-05652 Batch ID R37390 Test Code 8260OXYW Units pg1L Analysis Date 10/12/05 2 19 00 AM Prep Date <br /> Client ID Run ID ORGCMS3_051011B SegNo 538167 <br /> Anatyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual <br /> Methyt tert butyl ether(MTBE) 1907 1 0 200 0 953% 80 120 196 256% 20 <br /> Tert-butyl alcohol(TBA) 3838 10 400 0 959% 25 162 399 392% 20 <br /> Di-isopropyl ether(DIPE) 1932 1 0 200 0 966% 80 120 194 0592% 20 <br /> Ethyl tert-butyl ether(ETBE) 1822 1 0 200 0 91 1% 77 120 19 2 514% 20 <br /> Benzene 2035 050 200 0 102% 78 117 200 160% 20 <br /> Tert-amyl methyl ether(TAME) 17 93 1 0 200 0 896% 64 136 191 610% 20 <br /> Toluene 2086 050 200 0 104% 80 120 200 439% 20 <br /> Ethylbenzene 1963 0 50 200 0 982% 80 120 189 365% 20 <br /> m p-Xylene 4042 0 50 400 0 101% 80 120 39 0 368% 20 <br /> o-Xylene 1820 050 200 0 910% 80 120 186 220% 20 <br /> 1 4-Dichlorobenzene d4 1 12 010 100 0 112% 81 139 1 09 296% 20 <br /> Qualifiers ND Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits B-Analyte detected in the associated Method Blank <br /> J Analyte detected below quantitation]imus R-RPD outside accepted recovery limits <br />