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October 21, 2004 Lab ID STK436814-01 Customer ID 3-14626 Micheline Doyle Mpf Description 1707C-Final Discharge Sample Results - Organic Preparation Analysis Constituents Results PQL Units Note Method Date/ID Date/ID EPA 625 ACT 1 Pentachlorophenol ND 50 uglL 3520C 10/06/04 A225 10/13/2004 A02 Phenanthrene ND 10 ug/L 3520C 10/06/04 A225 10/13/2004 A02 Phenol ND 10 uglL 3520C 10/06/04 A225 10/13/2004 A02 Pyrene ND 10 ugIL 3520C 10/06/04 A225 10/13/2004 A02 Pyridine ND 10 ug/L 3520C 10/06/04 A225 10/13/2004 A02 1,2,4-Trlchlorobenzene ND 10 ug/L 3520C 10/06/04 A225 10/13/2004 A02 2,4,6-Trit,hlorophenol ND 10 ug/L 3520C 10/06/04 A225 10/13/2004 A02 1,2-Dlphenylhydrazine ND 50 ug/L 3520C 10/06/04 A225 10/13/2004 A02 EPA 8260B VOA 1 3 4-Brornofluorobenzene-Surrogate 92 1 56-126 % Rec 5030B 10/07/04 A233 10/08/2004 A02 Dibromotluoromethane-Surrogate 99 1 75-156 % Rec 50308 10/07/04 A233 10/08/2004 A02 1,2-Dichloroethane-d4-Surrogate 83 9 73-129 % Rec 5030B 10/07/04 A233 10108/2004 A02 Toluene-d8-Surrogate 94 9 85-109 % Rec 5030B 10/07/04 A233 10/08/2004 A02 Benzene ND 2 50 ug/L 5030B 10/07/04 A233 10/08/2004 A02 tert-Butanol ND 500 ug/L 5030B 10/07/04 A233 10/08/2004 A02 Di-isopropyl ether (DIPE) ND 50 ug/L 5030E 10/07/04 A233 10/08/2004 A02 Ethyl Benzene ND 2 5` ug/L 5030B 10/07/04 A233 10108/2004 A02 Ethyl tert-butyl ether (ETBE) ND 5• ug/L 5030B 10/07/04 A233 10/08/2004 A02 Methyl tert-butyl ether (MTBE) ND 50 ug/L 5030B 10/07/04 A233 10/08/2004 A02 tert-Amyl methyl ether (TAME) ND 5° ug/L 5030B 10/07/04 A233 10/08/2004 A02 Toluene ND 2 54 ug/L 5030B 10/07/04 A233 10/08/2004 A02 Xylenes ND 2511 ug/L 5030E 10/07/04 A233 10/08/2004 A02 ND=Non-Detect PQL=Practical Quantitation Limit 0 PQL adjusted for dilutions, concentrations dry weight reporting or limited sample Containers (VOA) VOA, (AGT) Amber Glass TFE-Cap Preservatives (1) Coot 4°C (3) HCl pH < 2 STK436814 Chemical Results Page 5