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• October 21, 2004 Lab ID STK436814 Micheline Doyle Kipf Customer 3-14626 Quality Control - Organic Constituent Method Date/ID Type Units Cone QC Data DQO Note CLS-1 3-Dtchloropropene 624 10/07/2004 A224 Blank ug/L ND <0 5 BS ug/L 1000 914% 77-135 BSD ug/L 1000 sa 0% 77-135 BSRPD ug/L 13 3% 510 3 410 624 10/07/2004 A 00-CCV ug/L 1000 84 1% 24-176 trans-1 3 Dtchloropropene 624 10/07/2004 A224 Blank ug/L ND <0 5 BS ug/L 1000 105% 75-140 BSD ug/L 1000 924% 75-140 BSRPD ug/L 130% 510 7 410 624 10/07/2004 A 00-CCV ug/L 1000 942% 50-150 Ethyl Benzene 624 10/07/2004 A224 Blank ug/L ND <0 5 BS ug/L 1000 83 5% 80-147 SSD ug/L 1000 699% 80-147 435 BSRPD ug/L 176% 517 3 410 624 10!07/2004 A 00-CCV ug/L 1000 840% 59-141 Fluorobeuzene-Surrogate 624 10/07/2004 A224 Blank ug/L 9 987 108% 70-130 BS ug/L 9 987 111% 70-130 SSD ug/L 9987 112% 70-130 624 10!0712004 A 00-CCV ug/L 9 987 117% 70-130 2-Hexanone 624 10/07/2004 A224 Blank uglL ND <5 BS ug/L 10 00 499% 50-150 435 BSD ug/L 10 00 552% 50-150 435 BSRPD uglL 100% 29127 624 10/07/2004 A 00-CCV uglL 5000 918% 50-150 Methyl tert-Butyl Ether (MTBE) 624 10/07/2004 A224 Blank ug/L ND <0 5 624 10/07/2004 A 00-CCV ug/L 40 00 120% 50-150 4 Methyl 2 pentanone (MIBK) 624 10/07/2004 A224 Blank uglL ND <5 BS ug/L 10 00 490% 50-150 435 BSD ug/L 10 00 524% 50-150 435 BSRPD ug/L 69% 510 8 624 10/07/2004 A 00-CCV ug/L 50 00 895% 50-150 Methylene Chloride 624 10/07/2004 A224 Blank ug/L ND <0 5 BS uglL 1000 122% 65-136 BSD ug/L 10 00 116% 65-136 BSRPD ug/L 5 1% 511 0 624 10/07/2004 A 00-CCV uglL 10 00 122% 60-139 Pentafluorobenzene-Surrogate 624 10/07/2004 A224 Blank ug/L 9 987 113% 70-130 BS ug/L 9 987 116% 70-130 BSD ug/L 9 987 120% 70-130 Report continued on next page STK436814 Quality Control Page 6