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Y) � . October 21, 2004 Lab ID STK436814 Micheline Doyle Kipf Customer 3-14626 Quality Control - Organic Constituent Method Date/ID Type Units Conc QC Data DQO Note Benzo(a)anthracene 35200 10/06/2004 A225 BSD ug/L 1000 772% 33-143 BSRPD ug/L 03% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 104% 80-120 Benzo(a)pyrene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 712% 28-131 BS ug/L 1000 740% 17-163 SSD ug/L 1000 743% 17-163 BS RPD ug/L 05% 5 30 0 625 10/13/2004 A 01-CCV mg/L 8000 105% 80-120 Benzo(b)fluoranthene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 742% 34-149 BS ug/L 1000 719% 24-159 BSD ug/L 1000 73 9% 24-159 BSRPD ug/L 26% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 100% 80-120 Benzo(g h,i)perylene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 800% 33 121 • BS ug/L 1000 840% D-219 BSD ug/L 1000 83 3% D-219 BSRPD ug/L 0 8% 5 30 0 625 10/13/2004 A of-CCV mg/L 8000 110% 80-120 Benzo(k)fluoranthene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 73 3% 34-127 BS ug/L 1000 749% 11-162 BSD ug/L 1000 76 8% 11-162 BSRPD ug/L 25% S 3 0 0 625 10/13/2004 A 01-CCV mg/L 8000 106% 80-120 4-Bromophenylphenylether 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 75 8% 40-126 BS ug/L 1000 73 7% 53-127 BSD ug/L 1000 799% 53-127 BSRPD ug/L 80% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 109% 80-120 Butylbenzylphthalate 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 69 1% 23-137 BS ug/L 1000 752% D-152 BSD ug/L 1000 753% D-152 BSRPD ug/L 0 1% 5 30 0 625 10/13/2004 A 01-CCV mg/L 8000 111% 80-120 4 Chloro-3 methylphenol 3520C 10/06/2004 A225 Blank ug/L ND <20 LCS ug/L 2000 675% 45-114 Report continued on next page STK436814 Quality Control Page 9