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October 21, 2004 Lab ID STK436814 Micheline Doyle Kipf Customer 3-14626 Quality Control - Organic Constituent Method Date/ID Type Units Cone QC Data DQO Note 2,4-DEnttrotoluene 3520C 10/06/2004 A225 LCS ug/L 1000 754% 35-132 BS ug/L 1000 74 1% 39-139 BSD ug/L 1000 807% 39-139 BSRPD ug/L 86% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 107% 80-120 2 6-Dmitrotoluene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 815% 46-135 BS ug/L 1000 770% 50-158 BSD ug/L 1000 83 2% 50-158 BSRPD ug/L 7 8% -.5300 625 10/13/2004 A 01-CCV mg/L 8000 110% 80-120 1 2-Diphenylhydrazine 3520C 10/06/2004 A225 Blank ug/L ND <50 LCS ug/L 1000 78 9% 42-126 BS ug/L 1000 802% 54-116 BSD ug/L 1000 84 1% 54-116 BSRPD ug/L 39 s 50 0 625 10/13/2004 A 01-CCV mg/L 8000 116% 80-120 bts(2-Ethylhexyl)phthalate 3520C 10/06/2004 A225 Blank ug/L ND <5 LCS ug/L 1000 817% 39-153 BS ug/L 1000 84 9% 8-158 BSD ug/L 1000 845% 8-158 BSRPD ug/L 04% 5 30 0 625 10/13/2004 A 01-CCV mg/L 8000 118% 80-120 Fluoranthene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 75 9% 44-126 BS ug/L 1000 766% 26-137 BSD ug/L 1000 792% 26-137 BSRPD ug/L 3 3% 5 30 0 625 10/13/2004 A 01-CCV mg/L 8000 110% 80-120 Fluorene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 1000 904% 46-126 BS ug/L 1000 780% 59-121 BSD ug/L 1000 842% 59-121 BSRPD ug/L 77% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 111% 80-120 2-Fluorobtphenyl-Surrogate 3520C 10/06/2004 A225 Blank ug/L 1000 74 9% 43-116 LCS ug/L 1000 75 8% 43-116 BS ug/L 1000 723% 43-116 SSD ug/L 1000 820% 43-116 625 10/13/2004 A 01-CCV mg/L 1000 101% 80-120 2-Fluorophenol-Surrogate 3520C 10/06/2004 A225 Blank ug/L 2000 657% 21-100 Report continued on next page STK436814 Quality Control Page 13