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rl 1 October 21, 2004 Lab ID STK436814 Micheline Doyle Kipf Customer 3-14626 Quality Control - Organic Constituent Method Date/ID Type Units Cone QC Data DQO Note 2 4 6 Trtbromophenol-Surrogate 3520C 10/06/2004 A225 Blank ug1L 2000 73 0% 10-123 LCS ug/L 2000 728% 10-123 BS ug1L 2000 772% 10-123 13SD ug/L 2000 809% 10-123 625 10/13/2004 A 01 CCV mg/L 2000 104% 80-120 1 2 4-Tnchlorobenzene 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 10100 68 3% 39-104 B5 ug/L 1000 595% 44-142 BSD ug/L 1000 666% 44-142 BSRPD ug/L 113% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 103% 80-120 2 4 6-Trichlorophenol 3520C 10/06/2004 A225 Blank ug/L ND <10 LCS ug/L 2000 673% 46-105 B5 ug/L 2000 630% 37-144 BSD ug/L 2000 71 7% 37-144 BSRPD ug/L 13 0% 530 0 625 10/13/2004 A 01-CCV mg/L 8000 101% 80-120 tert Amyl methyl ether (TAME) 5030B 10/07/2004 A233 Blank ug1L ND <2 MDL ug1L 2000 106% 50-150 QAMDL ug/L 2000 064 2 8260B 10/07/2004 A 00-CCV ug1L 5000 966% 50-150 Benzene 5030B 10/07/2004 A233 Blank ug/L ND <1 LCS ug/L 1 50 00 105% 68-131 MS ugIL 5000 105% 66-131 (SP 410337-02) MSD ug/L 50 00 104% 66-131 MSRPD ug/L 09% 514 6 8260E 10/07/2004 A 00-CCV ug/L 50 00 88 6% 70-130 4 Bromotluorobenzene Surrogate 5030E 10/07/2004 A233 Blank ug/L 25 00 I00% 56-126 LCS ug/L 2500 102% 56-126 MS ug/L 2500 101% 56-126 (SP 410337-02) MSD ug/L 2500 102% 56-126 MDL ug/L 2500 944% 50-150 QAMDL ug/L 2500 1 0 1 8260E 10/07/2004 A GI-CCV ug/L 2500 106% 70-130 tert-Butanol 5030B 10/07/2004 A233 Blank ug/L ND <20 MDL ug/L 10 00 245% 50-150 QAMDL ug/L 10 00 14 20 8260E 10/07/2004 A 00-CCV ug/L 2500 103% 50-150 Drtsoprupyl ether (DIPS) 5030B 10/07/2004 A233 Blank ug/L ND <2 MDL ug/L 2000 518% 50-150 QAMDL ug/L 2000 0 50 2 Report continued on next page STK436814 Quality Control Page 17