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December 15, 2004 Lab ID STK438223-01 <br /> • Customer ID 3-14626 <br /> Micheline Doyle Kipf Description 1707C - Final Discharge <br /> Sample Results - Organic <br /> Preparation Analysis <br /> Constituents Results PQL Units Note Method Date/ID Date/ID <br /> EPA 8260B VOA 1,3 <br /> 4-Bromofluorobenzene-Surrogate 93 3 82-115 % Rec 5030E 11/30/04 A233 11/30/2004 A02 <br /> Dtbromofluoromethane-Surrogate 102 87-140 % Ree 5030E 11/30/04 A233 11/30/2004 A02 <br /> 1,2-Dtehloroethane-d4-Surrogate - 110 75-143 % Rec, 5030B 11/30/04 A233 11/30/2004 A02 <br /> Toluene-d8-Surrogate 90 4 84-112 % Rec 5030B 11/30/04 A233 11/30/2004 A02 <br /> Benzene ND 0 5 ug/L 5030B 11/30/04 A233 11/30/2004 A02 <br /> tert-Butanol ND 5 ug/L 5030E 11/30/04 A233 11/30/2004 A02 <br /> Di-isopropyl ether (DIPE) ND 0 5 ug/L 5030B 11/30/04 A233 11/30/2004 A02 <br /> Ethyl Benzene ND 0 5 ug/L 5030B 11/30/04 A233 11/30/2004 A02 <br /> Ethyl tert-butyl ether (ETBE) ND 0 5 ug/L 5030E 11/30/04 A233 11/30/2004 A02 <br /> Methyl Cert-butyl ether (MTBE) ND 0 5 ug/L 5030B 11130!04 A233 11/30/2004 A02 <br /> tert-Amyl methyl ether (TAME) ND 0 5 ug/L 5030B 11/30/04 A233 11/30/2004 A02 <br /> Toluene ND 0 5 ug/L 5030B 1I/30/04 A233 11/30/2004 A02 <br /> Xylenes ND 1 ug/L 5030B 11/30/04 A233 11/30/2004 A02 <br /> ND=Non-Detect PQL=Practical Quantitation Limit ♦ PQL adjusted for dilutions, concentrations, dry weight reporting, or limited sample <br /> Containers (AGT) Amber Glass TFE Cap (VOA) VOA Preservatives (1) Cool 4°C, (3) HCl pH < 2 <br /> • STK438223 Chemical Results Page 4 <br />