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Wig <br /> Sequoia 404 N CA lane <br /> Walnut Creek, CA 9459$ <br /> 4 (925) 988-9600 <br /> 11) Analytical FAX(925)988-9673 <br /> Gettler Ryan,Inc -Dublin Project Unocal <br /> 6747 Sierra Court Suite J ProjectNumber Unocal#2859 Reported <br /> Dublin CA,94568 Project Manager Deanna L Harding 09-Mar-00 10 29 <br /> Total Metals by EPA 6000/7000 Series Methods - Quality Control <br /> Sequoia Analytical -Walnut Creek <br /> Reporting Spike Source °/oREC RPD <br /> Analyte Result Lurut Units Level Result %REC Lumts RPD Lumt Notes <br /> Batch 0003012-200.7 <br /> Blank(0003012-BLK1) Prepared 03-Mar-00 Analyzed 08-Mar-00 <br /> Ferrous Iron ND 0 010 mg/1 <br /> LCS(0003012-BS1) Prepared 03-Mar-00 Analyzed 08-Mar-00 <br /> Ferrous Iron 100 0 010 mg/1 100 100 80-120 <br /> LCS Dup (0003012-BSDI) Prepared 03-Mar-00 Analyzed 08-Mar-00 <br /> Ferrous Iron 112 0010 mg/I 100 112 80-120 113 20 <br /> Matrix Spike(0003012-MS1) Source W002475-01 Prepared 03-Mar-00 Analyzed 06-Mar-00 <br /> Ferrous Iron 690 0 010 m9/1 100 61 800 80-120 <br /> Matrix Spike Dup (0003012-MSDI) Source W002475-01 Prepared 03-Mar-00 Analyzed 06-Mar-00 <br /> Ferrous Iron 694 0 010 mg/l 100 61 840 80-120 0 578 20 <br /> 1a Analytical-Walnut Creek The results in this report apply to the samples analyzed in accordance Kith the chain of <br /> custody document This analytical report must be reproduced in its entirely <br /> Page 17 of 21 <br />