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Sequoia 680 Chesapeake Drive Redwood Cry CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> 4o4 N Wiget Lane Walnut Creek CA 94598 (510) 988-9600 FAX(510)988 9673 <br /> �Ily Analytical 819 Striker Avenue,Sucre 8 Sacramento CA 95834 (916) 921-9600 FAX(916)921 0100 <br /> Gettler Ryan/Geostraiegies Client ProjectIDFormer lbnacal 2859, 28005485 <br /> 6747 Sierra Court, Ste J Matrix Liquid <br /> Dubiin, CA 94568 <br /> ,Attention Deanna Harding Work Order # 9803391-07-10 Reported Mar i7, 1998 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte Phosphorus Total Dissolved Total Kjeldahl <br /> Salad Nitrogen <br /> OC Batch# IN031198365300A ING31198160100A IN031198351400A <br /> Analy Method EPA 365 3 EPA 160 1 EPA 351 4 <br /> Prep Method N A. N A. N A <br /> Analyst P Sandrock W Loo K Cesar <br /> MS/MSD # 980339003 980339110 980339110 <br /> Sample Conc 0 76 1200 13 <br /> Prepared Date 3/11/98 3/11/98 3/11/98 <br /> Analyzed Date 3/16/98 3/12/98 3/11/98 <br /> Instrument I D # MANUAL MANUAL MANUAL <br /> Conc Spiked 5 0 mg/L 500 mg/L 20 mg/L <br /> Result 41 1700 17 <br /> 4VS % Recovery 67 100 79 <br /> Dup Result 42 1700 18 <br /> MSD % Recov 69 100 $4 <br /> RPD 24 00 57 <br /> RPD Limit 0-20 0-20 0-20 <br /> LCS # LCS031198 LCS031198 LCS031198 <br /> Prepared Date, 3/11/98 3/11/98 3/11/98 <br /> Analyzed Date 3/16/98 3/12/98 3/11/98 <br /> Instrument I D.# MANUAL MANUAL MANUAL <br /> Conc. Spiked 0 50 mg/L 500 mg/L 100 mg/L <br /> LCS Result: 040 520 120 <br /> LCS % Recov 80 104 120 <br /> MSIMSD 75-125 75-125 75-125 <br /> LCS 80-120 80-120 80-120 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> Viiect <br /> EOUOIA ALYTICAL preparation,and analytical methods employed for the samples The matrix spike Is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fail within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> gory <br /> anager •*MS=Matrix Spike, MSD=MS Duplicate, RPO=Relative%Difference 9803390 GET <11> <br />