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M � 4 N Wget Lane Sequoia Walnut Crreek CA 94598 (925)988-9600 Analytical FAX(925)988-9673 Gettler Ryan,Inc -Dublin Project Unocal 6747 Sierra Court Suite J Project Number Unocal#2859 Reported Dublin CA,94568 Project Manager Deanna L Harding 09-Dec-99 15 07 Total Metals by EPA 6000/7000 Series Methods Sequoia Analytical -Walnut Creek Reporting Analyte Result Lunit Units Dilution Batch Prepared Analyzed Method Notes MW-1(W911614-02)Water Sampled 22-Nov-99 1.3 58 Received 22-Nov-99 20 00 Ferrous Iron 0 034 0 010 rng/l l 9LO3011 03-Dec-99 08-Dec-99 EPA 6010A MW-2(W911614-03)Water Sampled 22-Nov-9916 20 Received 22-Nov-99 20 00 Ferrous Iran 12 0 010 mg/l 1 9L03011 03-Dec-99 08-Dec-99 EPA 6010A MW-3(W911614-04)Water Sampled 22-Nov-991428 Received 22-Nov-99 20 00 Ferrous Iron 0 054 0 010 mg/1 1 9LO3011 03-Dec-99 08-Dec-99 EPA 6010A MW4(W911614-05)Water Sampled 22-Nov-991325 Received 22-Nov-99 20 00 Ferrous Iron 0 011 0 010 mg/l 1 9L03011 03-Dec-99 08-Dec-99 EPA 6010A MW-5(W911614-06)Water Sampled 22-Nov-9911 35 Received 22-Nov-99 20 00 Ferrous Iron ND 0 010 mg/1 1 91A3011 03-Dec-99 08-Dec-99 EPA 6010A MW-6(W911614-07)Water Sampled 22-Nov-991500 Received 22-Nov-99 20 00 Ferrous Iron ND 0 010 mg/l 1 9LO3011 03-Dec-99 08-pec-99 EPA 6010A ASOW-7(W911614-08)Water Sampled 22-Nov-9910 50 Received 22-Nov-99 20 00 imus Iron ND 0 010 mg/l 1 9LO3011 03-Dec-99 08-Dec-99 EPA 6010A MW-8(W911614-09)Water Sampled 22-Nov-99 12 10 Received 22-Nov-99 20 00 Ferrous Iron 0 015 0 010 mg/l 1 9LO3011 03-Dec-99 08-Dec-99 EPA 6010A MW-9(W911614-10)Water Sampled 22-Nov-991245 Received 22-Nov-99 20 00 Ferrous Iron ND 0 010 mg/l 1 9LO3011 03-Dec-99 138-Dec-99 EPA 6010A Sequoia Analytical-Walnut Creek The results rn tins reporr apply to the samples analyzed in accordance with the chain of custody document Thrs analytical report must be reproducedin ou entirety an p,La ratory Director Page 6 of 17