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* CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone (209) 384-2930 <br /> Certificate #2079 Fax (209) 384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Sampled 11-4-97 <br /> of Northern California Reference Number 1316 Received 11-5-97 <br /> 4005 N Wilson Way Sample Description Sail Extracted 11-5-97 <br /> Stockton, CA 95205 Sample Prep/Analysis Method EPA 5030/8015M, 8020 Analyzed 11-7-97 <br /> Attn Tim Cuellar Lab Numbers 1316-6S, 7S, 8S, 9S, 10S Reported 11-12-97 <br /> TOTAL PETROLEUM HYDROCARBONS - GASOLINE RANGE <br /> WITH BTEX DISTINCTION <br />' ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> AW2-35 AW2 45 AW2-60 AW2-70 AW2-80 <br /> (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) <br />' MTBE 0 010 ND ND ND ND ND <br /> BENZENE 00050 1 3 2 0 059 0 19 0 023 <br /> TOLUENE 00060 34 61 1 0 034 0 046 <br /> ETHYL BENZENE 00050 051 085 0 16 0 057 00079 <br />' TOTAL XYLENES 00050 26 4 0 075 027 0 037 <br /> GASOLINE RANGE <br /> HYDROCARBONS 1 0 22 56 98 3 2 ND <br /> Report Limit Multiplication Factor 5 10 1 1 1 <br /> Surrogate % Recovery NA NA FID 108%1 PID 102% FID 92 3%IND 90 1% FID 99 1%I PID 95 9% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> ANALYSTAPPROVED BY <br /> I aJCona�� Ja s Phi ip <br /> nvironmenta!Lab Director <br />