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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httn//www mccarnobell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 07/27/99 <br /> 4005 North Wilson Way Date Received 07/29/99 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 08102-08/04/99 <br /> Client P O Date Analyzed 08102-08104199 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 16278 16279 16280 16281 <br /> MW-8/7-27- MW-1217- MW-7/7-27- MW-4/7-27- Reporting Limit <br /> Client ID 99 27-99 99 99 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND ND<5 50 1 0 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND<5 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 37 so 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND<5 50 10 <br /> tert-Butanol ND ND ND ND<25 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 106 106 107 103 <br /> Comments <br /> 'water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis �` y uy <br /> Ihl hnhre.whwn. orer,m r,bte chem , Pm ! 1 I d c m le-a-co—an Pme1*1----—5.nl 0�sed—c-* /1 c .,. le d I ted d -•O <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />