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<br /> 110 Second Avenue South,#D7,Pacheco,CA 94553-5560
<br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> . bM2//www mccamlzb,ell,com E-mail main@mccampbell com
<br />' Advanced GeoEnvironmental Client Project 1D Cal Fuels Date Sampled 10/22/98
<br />' 4005 North Wilson Way
<br /> Date Received 10/27/98
<br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 10/30-11/05/98
<br />' CIient P O [Date Analyzed 10/30-11/05/98
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab ID 97744
<br /> Client 1D MW-11110-22-98
<br /> Matrix W
<br />' Compound Concentration* Compound Concentration
<br /> Acetone 86 Ethylbenzene ND
<br /> Benzene ND Hexachlorobutadwne ND
<br /> Bromobenzene ND lodomethane ND
<br />' Bromochloromethane ND Isopropyibenzene ND
<br /> Bromodichloromethane ND p-Isopropyl toluene ND
<br /> Bromoform ND Methyl butyl ketone` ' ND
<br /> Bromomethane ND Methylene Chloride" ND
<br /> n-Butyl benzene ND Methyl ethyl ketone` 3 1
<br /> sec-Butyl benzene ND Methyl isobutyl ketone 18 ND
<br /> tert-Butyl benzene ND Methyl tart-Butyl Ether(MTBE) ---
<br /> Carbon Disulfide ND Napthalene ND
<br /> Carbon Tetrachloride ND n-Propyl benzene ND
<br /> Chlorobenzene ND Styrene ND
<br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND
<br />' 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND
<br /> Chloroform 38 Tetrachloroethane 26
<br /> Chloromethane ND Toluene ND
<br /> 2-Chlorotoluene ND 1,2,3 Trichlorobenzene ND
<br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND
<br /> Dibromochloromethane ND 1,1,1-Tnchloroethane ND
<br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane ND
<br /> Dibromomethane ND Tnchloroethene ND
<br /> 1,2-Dichlorobenzene ND TnehlorOfluoromelhane ND
<br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchloropropane ND
<br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND
<br /> DichlorodifluoromethanL ND 1,3,5-Tnmethylbenzene ND
<br /> 1,1-Dichloroethane ND Vinyl Acetate m ND
<br /> 1,2-Dichloroethane ND Vinyl Chloride ND
<br /> 1,1-Dtchloroethene ND Xylenes,total ND
<br /> cis-1,2-Dichloroethene ND
<br /> trans-1,2-Dtchloroethene ND
<br /> 12-Dichloroproaane ND
<br /> l,3-Dichloropropane ND
<br /> 2,2-Dichloropropane ND Comments Br2FCH(Surrogate])not recovered due to matrix interference,
<br /> behavior confirmed by replicate analysis
<br /> 1,1-Dichloropropene ND Surrogate Recoveries(%)
<br /> cls-1,3-Dichloropropene ND Dibromofluoromethane ---
<br /> trans-1,3-Dichloropropene ND Toluene-d8 116
<br /> Ethylene dibromide ND 4-Bron,ofluorobenzene 96
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vnpe and all TCLP/SPLP extracts in uglL
<br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes
<br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol
<br /> sediment,0)sample diluted due to high organic content,(1,)peaks present in this carbon range do not match the pattem of our standard for
<br /> this analyte (1)methylbenzene (m)acetic acid cthenyl ester (n)chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 ward Hamilton, Lab Director
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