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�I <br /> l 110 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> b //www.mccamnbell ccs E-mail main@mccampbell com <br /> Advanced GeoEnvum <br /> onental Client Pradect ID Cal Fuels Date Sampled 10/22/98 <br /> 4005 North Wilson Way Date Received 10/27/98 <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 10/30-11/05/98 <br /> Client P O Date Analyzed 10/30-11/05/98 <br /> EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 97747 <br /> Client ID AW-213/10-22-98 <br /> Mat tx W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<7 Ethylbenzene ND <br /> IBenzene 220 Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chlonde" ND <br /> n-Butyl benzene ND Methyl ethyl ketone' ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone a ND <br /> tert-Butyl benzene ND Methyl tent-Butyl Ether(MTBE) ND <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> • Chlorobenzene ND Styrene ND <br /> Chloroethane ND 3,1,1,2-Tetrachloroethane ND <br /> 2-ChloroethyI Vmyl Ether` ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform 66 Tetrachloroethane ND <br /> Chloromethane ND Toluene` 24 <br /> 11 2-Chlorotoluene ND 1,2,3-Tnchi orobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane ND <br /> Dihromomethane ND Tnchloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchloropropane ND <br /> ],4-Dichlorobenzene ND 1,2,4-Trmethylbenzene ND <br /> Dichloroditluoromethant. ND 1,3,5-Tnmethylbenzene 56 <br /> 1,1-Dichloroethane ND Vinyl Acetate"' 52 <br /> 1,2-Dichloroethane 63 Vinyl Chloride`n ND <br /> I,1-Dichloroethene ND Xylenes,total `° 120 <br /> cis-1,2-Dichloroethene ND <br /> trans-],2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichlorapropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1 1-Dichloropropene ND Surrogate RecoN eries(%} <br /> cis-1,3-Dichloropropene ND Dibromotluoromethane 96 <br /> trans-],3-Dichloropropene ND Toluene-d8 115 <br /> Ethylene dibromide ND 4 Bromofluorobenzene 92 <br /> �tiratcr and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in uglL <br /> Reporting limits unless otherwise stated water samples l 0 ug/L, tapor samples 0 5 uglL, solid and sludge samples 5 ug/kg Hypes <br /> 0 2uglwipe ND means not detected abo%c the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 /% Edward Hamilton,Lab Director <br />