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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 44 htw//www mg;Amnbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 10/22/98 <br /> 4005 North Wilson Way <br /> Date Received 10/27/98 <br /> IStockton,CA 95205 Client Contact Tim Cuellar Date Extracted 10/30-11/05/98 <br /> Client P O Date Analyzed 10130-11105/98 <br /> Oxy enated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 97742 97743 97744 97745 <br /> MW-9/ MW_10/ MW-11/ MW-121 Reporting Limit <br /> Client 1D 10_22_98 10-22-98 10-22-98 10-22-98 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(RIPE) ND ND ND ND so 1 0 <br /> IEthyl tert-Butyl Ether(ETRE) ND ND ND ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND 4ND <br /> ND 50 10 <br /> tert-Butanol ND ND ND 25 50 <br /> Surrogate Reco%eries(%) <br /> Dibromofluoromethane 96 97 -- 94 <br /> IComments #Br2FCH(Surrogate 1)not recovered due to matnx interference, <br /> behavior confirmed by replicate analysis <br /> *water samples are reported in ug/L,soil and sludge samples to ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> I (h)lighter than water immiscible sheen is present,(i)liquid samplr that contains greater than—5 vol %sediment,{1)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 t��� Edward Hamilton, Lab Director <br />