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i <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> • 14 http//www mccamnbell com E-mail mainl✓mccampbell corn <br /> Date Sampled 07/16-07/17/98 <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels <br /> D <br /> 4005 North Wilson Way ate Received 07/22/98 <br /> Stockton,CA 95205 Client Contact Tim Cuellar Date Extracted 07/29/98 <br /> Client P O Date Analyzed 07129-07130198 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 92559 <br /> Client ID AW-213/7117!98 <br /> Matrix W <br /> Compound Concentration" Compound Concentration* <br /> Acetone ND<150 Ethylbenzene 81 <br /> Benzene 980 Hexachlorobutadiene ND<35 <br /> Bromobenzene ND<35 lodomethane ND<35 <br /> Bromochloromethane ND<35 Isopropylbenzene ND<35 <br /> Bromodichloromethane ND<35 p-Isopropyl toluene ND<35 <br /> Bromoform ND<35 Methyl butyl ketone` ND<35 <br /> Bromomethane ND<35 Methylene Chloride" ND<35 <br /> n-Butyl benzene ND<35 Methyl eihyl ketone" ND<35 <br /> sec-Butyl benzene ND<35 Methyl isobutyl ketone's ND<35 <br /> teri-Butyl benzene ND<35 Methyl teri-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<35 Napthalene ND<170 <br /> Carbon Tetrachloride NIK35 n-Propyl benzene ND<35 <br /> Chlorobenzene ND<35 Styrene' ' ND<35 <br /> Chloroethane ND<35 1,1,1,2-Tetrachloroethane ND<35 <br /> 2-Chloroethyl Vinyl Ether(c) ND<35 1 1,2 2-Tetrachloroethane ND<35 <br /> Chloroform ND<35 Tetrachlorocthene ND<35 <br /> Chloromethane ND<35 Toluene" 420 <br /> 2-Chlorotoluene ND<35 1 2 3-Trtchlorobenzene ND<35 <br /> 4-Chlorotoluene ND<35 1 2 4-Trtchlorobenzene ND<35 <br /> Dibromochloromethane ND<35 1 1 1-Ti ichloroethane ND<35 <br /> 1 2-Dibromo 3-chloropropane ND<35 1,1 2-Trichloroethane NIK35 <br /> Dibromomethane ND<35 Trichloroethene ND<35 <br /> 12-Dichlorobenzene ND<35 Trichlorotluorumethane ND<35 <br /> I 3-Dichlorobenzene ND<35 1 2 3-Trichloropropane ND<35 <br /> 1 4-Dichlorobenzene ND<35 1 2 4-Trimethylbenzene 84 <br /> Dichlorodifluoromethane ND<35 1 3 5-Trimethylbenzene ND<35 <br /> 1 1-Dicllloroethane ND<35 Vinyl Acetate"" ND<35 <br /> II 1 2-Diehl oroethane ND<35 Vinyl Chloride"' ND<35 <br /> 1,1-Dichloroethene ND<35 Xylenes,total `° 320 <br /> cis-1 2-Dichloroethene ND<35 <br /> trans-l2-Dichloroethene ND<35 <br /> 1 2-Dchloropropane ND<35 <br /> 1 3-Dichloropropane ND<35 <br /> 2 2-Dichloropropane ND<35 Comments <br /> 1,1-Dichloropropene ND<35 Surrogate 12eco%eries(1%) <br /> cts-13-Dichloropropene ND<35 Dibromotluoiomethane 108 <br /> trans-1,3-Dichloropropene ND<35 Toluene-d8 101 <br /> Ethylene dibromide ND<35 4-Bromofluorobenzene 110 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkg,%Sipes in ugh,.ipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (l)methylbenzene (m)acetic acrd ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 _Edward Hamilton,Lab Director <br />