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E <br /> CASTLE ANALYTICAL LABORATORY <br /> E Environmental Testing Services 2333 Shuttle Drive,Atwater CA 95301 Phone (209) 384-2930 <br /> Cartirlcate#1-2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal Fuels Sampled 12-19-01 <br /> E of Northern California Reference Number 4310 Received 12-20-01 <br /> 837 Shaw Road Sample Description Water Extracted 12-28-01 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 12-26-01 <br /> Attn Tim Cuellar Lab Numbers 4310-6W, 7W, 8W, 9W, 10W Reported 1-4-02 <br /> E <br /> EGASOLINE ADDITIVES BY EPA METHOD 3260 GCIMS <br /> ANALYTE REPORTING SAMPLE ID SAMPLE 0 SAMPLE ID SAMPLE ID SAMPLE ID <br /> E LIMIT MW 6 MW 7 MW 8 MW 9 MW 10 <br /> 121901 121901 121901 121901 121901 <br /> (Ng/L) (uglL) (uglL) (uglL) (ug/t} {ug/L) <br /> E FUEL OXYGENATES - <br /> Methyl tert-Butyl Ether(MTBE) 050 NO NO NO NO NO <br /> EDi-isopropyl Ether (DIPE) 0 50 ND NO NO NO NO <br /> Erhyl tert-Butyl E+her (ETRE) 050 NO NO NO ND NO <br /> tert-Amyl Methyl Ether(TAME) 050 NO NO NO NO NO <br /> tert-Butanol (TBA) 20 NO NO NO NO NO <br /> I <br /> EVOLATILE HALOCARBONS <br /> 1 2-Dichloroethane (1 2-DCA) 050 NO NO NO NO NO <br /> EE�hylene Dibromide (EDB) 050 NO NO NO NO NO <br /> EReport Limit Multiplication Factor 1 1 1 1 1 <br /> I <br /> ESurrogate Recoveries <br /> 1 2-Dichloroethane-d4 935% 112% 103% 105% 114% <br /> E Toiuene-d8 120% 115% 116% 118% 116% <br /> Instrument ID HP 5972MS <br /> Analytes reported as ND were not detected or below the Prac*ical Quantitation Limit <br /> E Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> (pglL)= micrograms per liter or parts per billion (ppb) <br /> C/"�'� - Al <br /> E ANALYST APPROVED BY <br /> Clan J Cone Ja s hdllps <br /> oratory Director <br /> I <br />