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I110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br />' 24 hhM//www mccampbell com E-mail mam@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels <br /> Date Sampled 09/19/01 <br /> 837 Shaw Road Date Received 09/20/01 <br /> Stockton,CA 95215 Client Contact Tun Cuellar Date Extracted 09/24-09/25101 <br /> Client P O Date Analyzed 09/24-09125101 <br /> Gasoline Range(C6-C12)Volatale Hydrocarbons as Gasohne*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA,methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br /> Lab ID Client ID Matrix TPH(g)+ MTBE Benzene Toluene Ethyl Xylenes %Recovery <br /> benzene Surrogate <br /> 78957 0001 W 350,a ND 067 4 4 ND ND 107 <br /> 78958 MW2/a919o1 W 2500,a ND<10 51 13 120 40 98 <br /> 78959 MW3/ W 34,000,a ND<100 3800 1900 1600 7300 103 <br /> 091901 <br /> 78960 MW4/ W 48,000,a ND<200 4400 1500 3400 11,000 102 <br /> 091901 <br /> 78961 MW51 W ND ND ND ND ND ND 105 <br /> 091901 <br /> I 78962 MW6/ W 660,a ND 3 5 5 8 3 0 ND 109 <br /> 091901 <br /> 78963 MW7/ W ND ND ND ND ND ND 103 <br /> 091901 <br /> 78964 MW8/ W ND ND ND ND ND ND 108 <br /> 09I901 <br /> 78965 MW9/ W 87,a ND ND 3 5 ND ND 110 <br /> I 091901 <br /> 78966 MW 10/ W ND ND ND ND ND ND 103 <br /> 091901 <br /> 78967 MWII/ W NO ND ND 052 ND ND 106 <br /> I 091901 <br /> 78968 MW12/ W ND ND ND ND ND ND 108 <br /> 091901 <br /> 78969 MW 13/ W 250,a ND ND 4 6 3 5 12 113 <br /> 091901 <br /> 78970 AWIA/ W 81,000,a ND<100 3200 8400 3800 17,000 ---# <br /> 091901 <br /> I Reporting Limit unless W 50 ug/L 5 0 0 5 0 5 0 5 05 <br /> otherwise stated,ND <br /> means not detected above <br /> the reporting limit S 1 0 mg/kg 0 05 0 005 0 005 0 005 0 005 <br /> "water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> #cluttered chromatogram,sample peak coelutes with surrogate peak <br /> I *The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br /> gasoline"), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant,biologically altered gasotinel,e)TPH pattern that does not appear to be denved from gasoline(1),f) <br /> one to a few isolated peaks present g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible <br /> sheen is present,i)liquid sample that contains greater than—5 vol %sediment j)no recognizable pattern <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />