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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ihtt»//www mccam bell co m E-mail main@mccampbell com <br /> iAdvanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 09/19/01 <br /> 837 Shaw Road Date Received 09/20/01 <br /> iStockton, CA 95215 Client Contact Tim Cuellar Date Extracted 09/28/01 <br /> i <br /> Lent <br /> P Q =DateAnalyzed 09/28/01 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> i Lab ID 78957 78958 78959 78960 <br /> MWl/ MW2/ MW31 MW4/ Reporting Limit <br /> Client ID 091901 091901 091901 091901 <br /> iMatrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> iDi-isopropyl Ether(DIPS) ND ND ND<10 ND<20 50 10 <br /> iEthyl tert-Butyl Ether(ETBE) ND ND ND<10 ND<20 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND<10 ND<20 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<10 ND<20 50 10 <br /> itent-Butanol ND ND ND<50 ND<100 25 50 <br /> iSurrogate Recoverics(%) <br /> iDibrotnofluoromethane 106 120 118 117 <br /> Comments <br /> i *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> i (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> i <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> i <br /> i <br />