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I <br /> 110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> I McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hM//www mcc,ampbeli coin E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 12/21/00 <br /> 4005 North Wilson Way Date Received 12/27/00 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 12/27-01102/01 <br /> I Client P O Date Analyzed 12/27-01/02/01 <br /> Oxygenated Volatile Organics By GC/MS <br /> LEP=A..t=hod8260 modified <br /> Lab M 56934 56935 56936 56937 <br /> AW1A/ AW1B/ AW2A/ AW2B/ Reporting Limit <br /> Client ID 122100 122100 122100 122100 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND<50 ND<10 ND<63 ND<10 50 1 0 <br /> Ethyl tent-Butyl Ether(ETBE) ND<50 ND<10 ND<63 ND<10 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND<50 ND<10 ND<63 ND<l0 5 0 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<50 ND<10 INND<63 ND<10 5 0 1 0 <br /> tent-Butanol ND<250 ND<50 3 ND<50 25 50 <br /> Surrogate Recoveries(%) <br /> Dihromotluoromethane 102 103 102 103 <br /> Comments J J t 3 <br /> I *water samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC I SDLP extracts in ug/L <br /> ND means not detected above the reporting limit.NIA means surrogate not applicable to this analysts <br /> I (h)lighter than water immiscible sheen is present (t)liquid sample that contains greater than—5 vol %sediment (I)sample diluted due to <br /> high organic content <br /> I <br /> DIIS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br /> I <br />