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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> I McCAMPBELL ANALYTICAL INC 'Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 hap//www mocampbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Cal Fuels Date Sampled 08/16/00 <br /> 4005 North Wilson Way Date Received 08/25/00 <br /> IStockton, CA 95205 Client Contact Tim Cuellar Date Extracted 08/25/00 <br /> Client P O Date Analyzed 08/25-08/28100 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 45872 45873 45874 45875 <br /> Reporting Limit <br /> Client ID MW 13-15 MW 13-20 MW 13-25 MW 13-35 <br />' Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L. <br /> IDi-isopropyl Ether(DIPS) ND ND ND<l 00 ND<10 50 1 0 <br /> I Ethyl tert-Butyl Ether(ETRE) ND ND ND<100 ND<10 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND<100 ND<10 50 l 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND<100 ND<10 50 1 0 <br /> tent-Butanol ND ND ND<500 N13<50 25 50 <br /> IMethanol ND ND ND<20,000 ND<2000 1000 200 <br /> Ethanol ND ND ND<5000 ND<500 250 50 <br /> ISurrogate Recoveries(%) <br /> Dibromofluoromethane 92 93 98 88 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L. <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(1)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> • <br />