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CASTLE ANALYTICAL LABORATORY <br />' Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br />' Advanced GeoEnvironmental Inc Client Project ID Cal-Fuels Sampled 01-20-03 <br /> of Northern California Reference Number 5400 Received 01-22-03 <br /> 837 Shaw Road Sample Description Soil Extracted 01-27-03 <br /> Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8015M 8020 Analyzed 01-27-03 <br />' Attn Tim Cuellar Lab Numbers 5400-1 S,2S, 3S,4S Reported 02-06-03 <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE RANGE <br />' WITH BTEX DISTINCTION <br />' ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> EW1 -20 EW1 -35 EW1 -50 EW1 -65 <br /> (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) <br /> MTBE 0 010 ND ND ND ND <br />' BENZENE 00050 NO 12 0 053 ND <br />' TOLUENE 00050 ND 220 027 ND <br /> ETHYLBENZENE 00050 ND 75 0 091 ND <br /> I • TOTAL XYLENES 00050 68 370 048 00078 <br /> GASOLINE RANGE <br /> HYDROCARBONS 10 2700 3300 38 ND <br />' Report Limit Multiplication Factor 500 500 1 1 <br /> Surrogate% Recovery NA NA F10 823,61 PID 883% Flo 735A/PTD 745% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> IPractical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST �✓r.' " �f APPROVED BY <br /> Clan J Cone �' /a hdlrps <br /> ' p6oratory Director <br />