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' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive Atwater CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Project ID Cal-Fuels Sampled 01-20-03 <br /> of Northern California Reference Number 5400 Received 01-22-03 <br /> 837 Shaw Road Sample Description Sod Extracted 01-23-03 <br />' Stockton CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 01-23-03 <br /> Attn Tim Cuellar Lab Number 5400-2S Reported 02-06-03 <br /> Client Sample ID EW 1 -35 <br /> VOLATILE ORGANICS -EPA METHOD 8260 GCIMS <br /> REPORTING SAMPLE REPORTING SAMPLE; <br /> I ANALYTE LIMIT* RESULT ANALYTE LIMIT" RESULT <br /> (mlk ) (mg/kg) (mg/kg) m <br /> Benzene 0 010 15 1,3-Drchloro ro ane 0 010 NO <br /> Bromobenzene 0 010 NO 2 2-Drchloro ro ane 0 010 NO <br /> Bromochloromethane 0 010 NO 1,1-Drchloro ro ene 0 010 ND <br /> Bromodichloromethane 0 010 NO cis-1 3-Drchloro ro ene 0 010 ND <br /> Bromoform 0 010 ND trans-l,3-Drchloro ro ene 0 010 ND <br /> Bromomethane 0 010 NO Eth (benzene 0 010 84 <br /> n-Bu! lbenzene 0 010 11 Hexachlorobutadiene 0 010 NQ <br /> sec-But lbenzene 0 010 37 isopropylbenzene 0 010 81 <br /> tert-But lbenzene 0 010 NQ -Isopropyl toluene 0 010 2 2 <br /> Carbon tetrachloride 0 010 NO Methylene chloride 0 040 ND <br /> Chlorobenzene 0 010 NO Methyl tert-Bu! I Ether(MTBE) 0 010 NO <br /> Chlorodibromomethane 0 010 NO Na thalene 0 040 39 <br /> Chloroethane 0 010 NO n-Propylbenzene 0 010 26 <br /> Chloroform 0 010 NO Styrene 0 020 NO <br />� . Chloromethane 0 010 NO 1,1,1,2-Tetrachloroethane 0 010 NO <br /> 2-Chlorotoluene 0 010 NO 1,1,2 2,-Tetrachlore+hane 0 010 ND <br /> 4-Chlorotoluene 0 010 NQ Tetrachloroethene 0 010 NO <br /> 1 2-Dibromo-3-chloroero ane 0 020 NO Toluene 0 010 270 <br /> 1 2-Dibromoethane(EDB) 0 010 NO 1,2,3-Trichlorobenzene 0 010 NO <br /> Dioromomethane 0 010 NO 1 2 4-Trichlorobe nzene 0010 NO <br /> 1 2-Dichlorobenzene 0 010 <br /> NO 1 1 1-Trichloroethane 0 010 NO <br /> 1 3-Dichlorobenzene 0 010 NO 1 1,2-Trichloroethane 0 010 NO <br /> 1 4-Dichlorobenzene 0 010 NO Trichloroethene 0 010 NO <br /> Dichlorodifluoromethane 0 010 NO Trichlorofluoromethane 0 010 NO <br /> 1 1-Dichloroethane 0 010 ND 1 2 3-Trichlora ro pane 0 010 ND <br /> 1 2-Dichloroethane 0 010 NO 1 2 4-Tnmeth lbenzene 0 010 160 <br />' 1 i-Drchloroethene 0 010 ND 1 3,5-Tnmeth lbenzene 0 010 44 <br /> cis-1 2-Drchloroethene 0 010 ND Vinyl Chlonde 0 010 NO <br /> trans-1 2-Dichloroethene 0 010 ND Xylenes, total 0 010 440 <br /> 1,2-Drchloro ro ane 0 010 ND <br /> *Report Limit Multiplication Factor 100* <br /> *Report Limit Multiplication f=actor for Toluene 200 <br /> **Re ort hmrt raised due to matrix interference <br /> Surrogate Recoveries <br /> Dibromofluoromethane NA Toluene-d8 NA <br /> 1 2-Dichloroethane-d4 NA p-Bromofluorobenzene NA <br /> Instrument ID HP 5972MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit= Reporting Limit x Report Limit Multiplication Factor <br /> mg/Kg = milligra s per kdogram,9"arts{per million(ppm) <br /> i I , Jff <br /> ANALYST �' - APPROVED BY <br /> Clara J Cone _ acnes C Phillips <br /> Laboratory Director <br />