Laserfiche WebLink
CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive Atwater CA 95301 Phone (209)384-2930 <br /> Fax (209)384-1507 <br /> Advanced GeoEnvironmental Inc Client Project ID Cal-Fuels Method EPA 5030/8260 <br /> of Northern California Reference Number 5400 Instrument ID HP Series II <br /> 837 Shaw Road Matrix Sail Prepared 01-23-03 <br /> Stockton CA 95215 Analyst Scott Foster Analyzed 08-23-02 <br /> Attn Tim Cuellar Reported 02-06-03 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID VSMS-1223 <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> m IK mg/K mg/K %R <br /> COMPOUNDS <br /> I t-But l Alcohol(t-BA) 080 ND 300 994% 70-130 <br /> Methyl t-but I ether (MTBE) 001 ND 0 100 864% 70-130 <br /> Duso rop I ether(DIPE) 001 ND 0 100 106% 70-130 <br /> Ethyl t-But I ether(ETBE) 001 ND 0 100 108% 70-130 <br /> t-Am 1 methyl ether TAME 001 ND 0 100 864% 70-130 <br /> 1,2-Dichloroethane(1 2-DCA) 001 ND 0 100 888% 70-130 <br /> Ethylene dibromide(EI]B) 001 NO 0 100 864% 70-130 <br /> 1 1-Dichloroethene(1 1 DCE) 001 NO 0 100 105% 70-130 <br /> I Benzene 001 NO 0 100 952% 70-130 <br /> Trichloroethene (TCE) 001 ND 0 100 840% 70-130 <br /> Toluene 001 ND 0 100 107% 70-130 <br /> Chlorobenzene 001 ND 0 100 896% 70-130 <br /> Surrogate <br /> t7ibromofluoromekhane 0 010 140% 0 400 1150/0 70-130 <br /> 1 2-Dichloroethane-d4 0 010 135% 0 400 978% 70-130 1 <br /> Toluene-d8 0 010 108% 0 400 101% 70-130 <br /> 4-Bromorluorobenzene 0 010 1114/0 0 400 108% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP L mats <br /> mg/Kgmg/Kg %R %R <br /> COMPOUNDS <br /> t-Butyl Alcohol(t-BA) 300 994% 113% 70-130 130% <br /> Methyl t-but l ether (MTBE) 0 100 864% 788% 70-130 920% <br /> Diisopro l ether(DIPE) 0 100 106% 112% 70-130 588% <br /> Ethyl t-But I ether(ETBE) 0 100 1080/6 105% 70-130 264% <br /> t-Am I methyl ether(TAME) 0 100 864% 892% 70-130 319% <br /> 1 2-Dichioroethane(1,2-DCAJ 0 100 888% 856% 70-130 367% <br /> Ethylene dibromide(EDB) 0 100 864% 892% 70-130 319% <br /> 11-DEchloroethene01,DCE) 0100 105% 109% 70-130 375% <br /> Benzene 0 100 952% 102% 70-130 729% <br /> Trichloroethene(TCE) 0 100 840% 932% 70-130 104% <br /> Toluene 0 100 107% 115% 70-130 719% <br /> Chlorobenzene 0 100 896% 960% 70-130 690% <br /> Surrogate <br /> Dtbromofluoromethane 0 400 115% 118% 70-130 232% <br /> 1,2-Diichloroethane-d4 0 400 978% 108% 70-130 973% <br /> Toluene-d8 0 400 101% 106% 70-130 473% <br /> 4-Bromofluorobenzene 0 400 1080/. 110% 70-130 183% <br /> t The LCS(Laboratory Check Sample) is a control sample of known interferent free matrix that is fortified with representative analytes and <br /> i1 analyzed using the same reagents, preparation and analytical methods employed for the samples The LCS.% recovery is used for validation <br /> of sample batch results Due to matrix effects,the QC limits and recoveries for MSIMSD's are advisory only and are not used to accept or <br /> reject batch results <br /> I J l <br /> ANALYST �n APPROVED B)aborma�tory <br /> Clar Cone sPhillips <br /> Director <br />