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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www meeampbell coin E-mail main@mccampbell coin <br /> • <br /> Advanced GeoEnvironmental Client Project ID Pacific Mini Mart Date Sampled 03/20/02 <br /> 837 Shaw Road Date Received 03/20/02 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 03/20/02 <br /> Client P O Date Analyzed 03/20/02 <br /> LUFT Metals* <br /> EPA analytical methods 6010/200 7,239 2' <br /> Lab ID Client ID Matrix Extraction' Cadmium Chromium Lead Nickel Zinc %Recovery <br /> Surrogate <br /> 0203358- Effluent W TTLC ND ND ND ND ND 105 <br /> 0022 <br /> I <br /> S TTLC 0 5 mg/kg 05 30 20 10 <br /> Reporting Liritit unless <br /> otherwise stated,ND W TTLC 0 005 mg/L 002 0 005 005 005 <br /> means not detected above <br /> the reporting limit STLC, <br /> -- 4 01 mg/L 0 05 4 2 0 OS 0 45 <br /> TCLP <br /> *water samples are reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts to mg/L <br /> "Lead is analysed using EPA method 6010(ICP)for soils,STLC&TCLP extracts and method 239 2(AA Furnace)for water samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,T7LC),STLC-CA Title 22 <br /> DISTLC extractions are pertormed using STLC methodology except that deionized water is substituted for citric acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> s reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than —2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />