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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAAPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Arco Mini Mart Date Sampled 02/15/2002 <br /> 837 Shaw Road (Pacific) Date Received 02/18/2002 <br />' Stockton, CA 95215 Client Contact Bill Little Date Extracted 02/21-02/2712002 <br /> Client P O Date Analyzed 02/21-02/27/2002 <br /> Seven Oxygenated Volatile Organics By GCIMS <br /> EPA method 8260 modified <br /> Lab ID 90613 90614 90615 90616 <br /> MW11A102 MWl IB/021 MW12A/02 MW2B/0215 Reporting Limit <br /> Cheat ID 1502 502 1502 02 <br />' Matnx W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPE) ND<10 ND<5 0 ND<5 0 ND 50 10 <br />' Ethyl tent-Butyl Ether(ETBE) ND<10 ND<5 0 ND<5 0 ND 50 10 <br /> Methyl tart-Butyl Ether(MTBE) 520 220 330 84 50 10 <br /> 1 <br /> tent-Amyl Methyl Ether(TAME) ND<10 ND<5 0 ND<5 0 ND 50 10 <br />' tert-Butanol ND<50 ND<25 ND<25 ND 25 50 <br />' Methanol ND<5000 ND<2500 ND<2500 ND 2500 500 <br /> Ethanol ND<500 ND<250 ND<250 ND 250 50 <br /> Surrogate Recoveries <br />' Dtbromofluoromethane 106 108 108 107 <br /> Comments <br /> *water samples are repotted in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SDLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(1)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> i <br />