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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell cam E-mail main@mccampbell com <br />' Advanced GeoEnvironmental CIient Project ID Pacific Mini Mart Date Sampled 12/10/01 <br />' 837 Shaw Road Date Received 12/11/01 <br /> Stockton, CA 95215 Client Contact Bill Tattle Date Extracted 12/11/01 <br /> [Client P O Date Analyzed 12/11/01 <br /> LUFT Metals* <br /> EPA analytical methods 6010/200 7,239 2* <br />' Lab ID Client ID Matrix Extraction' Cadmium Chromium Lead Nickel Zinc %Recovery <br /> Surrogate <br /> 85714 Influent W TTLC ND ND ND ND ND 109 <br /> 85715 Effluent W TTLC ND ND ND ND ND 104 <br /> I• <br /> Reporting Larat unless S TTLC 0 5 mg/kg 05 30 20 10 <br /> otherwise stated ND W TTLC 0 005 mg/L 002 0 005 005 005 <br /> means not detected above <br /> the reporting limit STLC, <br /> -- TCLP 0 01 mg/L 005 02 005 005 <br /> *water samples are reported in mg/L,soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in mg/L <br /> "Lead is analysed using EPA method 6010{ICP,fbr soils,STLC&TCLP extracts and method 239 2(AA Furnace)for water samples <br /> 'EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(orgame matnces,TTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> r9 DISTLC extractions are performed using STLC methodology except that demnized water is substituted for citric acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> "surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> $reporting limit raised due to matrix interference <br /> . i) liquid sample that contains greater than —2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />