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4 <br /> MATRIX SPIKE SAMPLE DATA REPORT <br /> GC/MS Volatiles <br /> Client Lot #. . EOK170197 Work Order #- - - = DP2DVlAE-MS Matrix. . . . . . . . . : WATER <br /> MS Lot-Sample #: EOK160351-020 DP2DVIAF-MSD <br /> Date Sampled. . . : 11/16/00 14 15 Date Received. . : 11/16/00 17 00 MS Run #. . . . . . . : 0326235 <br /> Prep Date. . . . . . : 11/21/00 Analysis Date. . : 11/21/00 <br /> Prep Batch #_ . : 0326394 Analysis Time. . : 06 33 <br /> Dilution Factor: 1 <br /> SAMPLE SPIKE MEASRD PERCENT <br /> PARAMETER AMOUNT AMT AMOUNT UNITS RECOVERY RPD METHOD <br /> Benzene ND 10.0 8.74 ug/L 87 SW846 8260B <br /> ND 10.0 8.77 ug/L 88 0.34 SW846 8260B <br /> Chlorobenzene ND 10.0 8-32 ug/L 83 SW846 8260B <br /> ND 10.0 8.48 ug/L 85 1.9 SW846 8260E <br /> l,l-Dichloroethene ND 10.0 9.28 ug/L 93 SW846 8260B <br /> ND 10 0 9.19 ug/L 92 0.97 SW846 82608 <br /> Toluene ND 10.0 9.02 ug/L 90 SW846 8260E <br /> ND 10.0 9.02 ug/L 90 0.0 SW846 8260B <br /> Trichloroethene ND 10 0 8.70 ug/L 87 SW846 8260E <br /> ND 10.0 8.67 ug/L 87 0.34 SW846 8260B <br /> PERCENT RECOVERY <br /> &URROGATE RECOVERY LIMITS <br /> Bromofluorobenzene 106 (75 - 120) <br /> 104 (75 - 120) <br /> 1, 2-Dichloroethane-d4 114 (65 - 130) <br /> 111 (65 - 130) <br /> Toluene-d8 103 (80 - 130) <br /> 102 (80 - 130) <br /> NOTE(S) : <br /> Calculations are performed before rounding to avoid round-off errors to calculated results <br /> Bold print denotes control parameters <br /> 000035 <br />