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0 UAL I T Y C O N T R O L R E S U L T S <br /> Job Number 992528 Report Date 12/14/1999 <br /> CUSTOMER IT Group PROJECT Southland - Martinez ATTN Rhonda Teichetra <br /> QC Type Description Reag Code Lab 10 Dilution Factor Date Time <br /> MS Matrix Spike 09112901 992528-112,108/1999 0424 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> 1 <br /> 2-Dichloroethane 12 95 10 000000 0 44 125 1 70-130 <br /> ,2-Dibromoethane (EDB) 8 20 10 000000 0 82 0 70-130 <br /> MSD Matrix Spike Duplicate 09112901 992528-1 12/08/1999 0453 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> t <br /> ert-Butyl Alcohol (TBA) 1193 18 1129 43 1000 000000 0 119 3 34-182 <br /> 5 19 <br /> i-Isopropyl Ether 42 84 46 66 50 000000 0 85 7 60-131 <br /> 9 24 <br /> Ethyl tert-Butyl Ether (ETBE) 51 50 52 57 50 000000 0 04 102 9 64-138 <br /> 2 29 <br /> Itert-AmyL Methyl Ether 48 87 51 06 50 000000 0 97 7 67-154 <br /> 4 27 <br /> &L-t-Butyt Ether (MTBE) 135 09 133 00 100 000000 5 47 129 6 71-142 <br /> 2 31 <br /> ichloroethane 12 81 12 95 10 000000 0 44 123 7 70-130 <br /> 1 30 <br /> 1,2-Dibromoethane (EDB) 8 68 8.20 10 000000 0 86 8 70-130 <br /> 6 30 <br /> LCS Laboratory Control Sample 09120705 12/08/1999 0943 <br /> Parameter/Test Description QC Result QC Result True Value brig Value Calc Result * Limits F <br /> itert-ButyL Alcohol (TBA) 1332 01 1000 000000 133 2 37-175 <br /> Di-Isopropyl Ether 44 30 50 000000 88 6 60-138 <br />,EthyL tert-Butyl Ether (ETBE) 52 93 50 000000 105 9 51-143 <br /> tert-Amyl Methyl Ether 51 17 50 000000 102 3 64-137 <br /> Methyl-t-Butyl Ether (MTBE) 142 47 100 000000 142 5 33-169 <br /> 1,2-Dichloroethane 13 60 10 000000 136 0 70-130 X <br /> 1,2-Dibromoethane (EDB) 8 01 10 000000 80 1 70-130 <br /> 1 <br /> MB Method Blank 12/08/1999 1011 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br />�tert-Butyl Alcohol (TBA) 0 <br /> Di-Isopropyl Ether 0 <br /> Ethyl tert-Butyl Ether (ETBE) 0 <br /> tert-Amyl Methyl Ether 0 <br /> Methyl-t-Butyl Ether (MTBE) 0 <br /> 1,2-Dichloroethane 0 <br /> 1,2-Dibromoethane (EDB) 0 <br /> 0 <br />' Page 18 " X=X REC, R=RPD, A=ABS Diff., D=% Diff <br />