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_ _ _ _ R _ :.r <br /> ' t R <br /> c <br /> } <br /> AJ <br /> 1 <br />,Y <br /> E D- OX <br /> A 55n CIA li S ItJ<' <br /> MAGE 59 OF 61 <br /> . DATE EXTRACTED: 05/03/91 <br /> MED-TOX JOB N0: 9105035 <br /> DATE ANALY'LEP' 05/08/91 INSTRUMENT: 11 <br /> SAMPLE SPIKED: POLAR WATER <br /> MATRIX SPIKE RECO"7RY SUMMARY <br /> METHOD 8270 <br /> (WATER MATRIX) <br /> Ave rale <br /> Spike sa-ple Result Result Percent APD <br /> Result (ug/0 Recovery <br /> (ug/ /L) L) <br /> c) (Ug/0 Cug <br /> ANALYTE --- <br /> 56.3 10.9 <br /> 150 63.0 54.5 <br /> RD 62.6 39.4 14.4 <br /> Phenol <br /> 149 RD 49.8 36.8 10.8 <br /> 2-Chlorophenol X43 ND 55.5 70 1 46.8 5.5 <br /> 1,4-Dichlorobenzene ND 74.1 40-2 5.6 <br /> N-Nitroso-di-n-Propylamine 154 152 No 62.8 59.4 51.3 1.7 <br /> 1,2,4-Trichlorobenzene ND 51.6 73,8 75.1 2.7 <br /> t enol 145 74.3 76-4 <br /> 4-Chloro-3-methy Ph. 146 ND 107.0 72.1 4.7 <br /> Acenaphthene 145 ND 102.0 Bo.4 6.5 <br /> 4-Nitrophenol ND 93.3 99.6 73.5 2 5-4 <br /> 2,4-Dinitrotoluenc 120 109.0 115.0 153 RD 93. 2.8 <br /> lentechlaroplwnol 153 ND 145-0 141.0 <br /> Pyrene <br /> CURRENT QC LIMITS <br /> percent Recover RPO <br /> Analyte <br /> (12- 89) 42 <br /> Phenol (21 -123) 40 <br /> 2-Chlorophenol (36- 97) 28 <br /> 1,4--Dichlorobenzene 41_116) 38 <br /> N--Nitroso-di-n-propylamine (39- 98) 28 <br /> 1,2,4-Tri.chlorobenzene 23- 97) 42 <br /> 4-Chloro-3-methylphenol (46-118) 33 <br /> Acenaphthene (10- 80) 50 <br /> .4-Nitrophenol (24- 96) 38 <br /> 1,4-Dinitrotoluene ( 9-103) 50 <br /> Pentachlorophenol (26_127) 31 <br /> pyrene <br /> MS r Matrix Spike <br /> MSD = Matrix Spike Duplicate <br /> RPD = Relative Percent Difference <br /> ND = Not Detected <br />