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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 44 http//www mccampbell coin E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Tracy Marine Date Sampled 03/23/02 <br /> 837 Shaw Road Date Received 03/26/02 <br /> IStockton, CA 95215 Client Contact Brian Millman Date Extracted 03/28/02 <br /> [Clientpo Date Analyzed 03/28/02 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' <br /> Lab ID 0203458- 0203458- 0203458- 0203458- <br /> 005 006 007 008 Reporting Limit <br /> Client ID MW5/ MW6/ MW7/ MW8/ <br /> 032302 032302 032302 032302 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND<10 ND ND<500 ND so 10 <br />' Ethyl tert-Butyl Ether(ETRE) ND<10 ND ND<500 ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) 480 ND 41,000 3 6 50 1 0 <br /> tert-Amyl Methyl Etlier(TAME) ND<10 ND ND<500 ND 50 1 0 <br />' tert-Butanol ND<l00 ND ND<5000 ND 25 50 <br />' Surrogate Recoveries(%) <br /> Dibromofluoromethane 104 105 101 106 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting€nrut,NIA means surrogate not applicable to this analysis <br /> 1 (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />