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110 Second Avenue South,##D7, Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccamobell co m E-mail main@mccampbell com <br /> Advanced GeoEnviromnental Client Protect ID TMS <br /> Date Sampled 06/24/98 <br /> 4005 North Wilson Way Date Received 06/25/98 <br />' Stockton, CA 95205 Client Contact Bill Little Date Extracted 06/25-07/06/98 <br /> CIient P O Date Analyzed 06/25-07/06/98 <br /> I Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 91053 <br /> Client ID B3-H2O <br />' Matrix W- <br /> Compound Concentration* Compound Concentration* <br />' Acetone" ND<10 Ethylbenzene 240 <br /> Benzene 340 HCxaChlOiobutadiene ND<10 <br /> Bromobenzene ND<10 lodomethane ND<10 <br /> Bromochloromethane ND<10 Isopropylbenzene 16 <br />' Bromodichloromethane ND<10 p-lsopropyl toluene ND<10 <br /> Bromoform ND<10 Methyl butyl ketone' ' ND<10 <br /> Bromomethane ND<10 Methylene Chloride"' ND<10 <br /> n-Busy]benzene 16 Methyl ethyl ketone" ND<10 <br />' sec-Butv1 benzene ND<10 Methyl isobutrl ketone's ND<10 <br /> ten-Butyl benzene ND<10 Methyl Cert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<10 Napthalene ND<70 <br /> Carbon Tetrachloride ND<10 n-Propyl benzene ND<10 <br /> lieChlorobenzene ND<10 Styrene'" ND<10 <br /> Chloroethane ND<10 I l 1 2-Tetrachloroethane ND<10 <br /> 2-Chloroethyl Vinyl Ether` ND<10 1,1 2 2 Tetrachloroethane ND<10 <br /> Chloroform ND<10 Tetrachloioethene ND<10 <br /> I Chloromethane ND<10 Toluene" 24 <br /> 2-Chlorotoluene ND<10 1 2 3-Ti ichlowbenzene ND<10 <br /> 4-Chlorotoluene ND<10 1 2 4-Ti ichlorobenzene ND<10 <br /> Dibromochloromethane ND<10 1,1 1-Ti ichlomethane ND<10 <br /> 12-Dibromo-3-chloiopropane ND<10 1,12 fnchloroethane ND<10 <br /> Dibromomethane ND<10 Trichloroethene NIK10 <br /> 12-Dichlorobenzene ND<10 Trichlorolluaioniethane ND<10 <br /> 1 3-Dicliloroben2ene ND<10 1 23 Tsichloropropane ND<10 <br />' 1 4-Dichlorobenzene ND<10 1 2 4-Trime1h)/benzene 350 <br /> Dieh lorodltlUOTOnielhane ND<10 1,3,5-Tnmc1hvlbcn7ene 120 <br /> 1,1-Dichloroethane ND<10 VmvlAcetate""' 13 <br /> 1,2-Dichloroethane ND<10 Vtnvl Chloiide"I ND<10 <br />' 1 I-Dichloroethene ND<10 Xylenes total '°' 820 <br /> cis-1 2-Dicliloroethene ND<10 <br /> tians-1 2-Dichloroethene ND<10 <br />' 1,2-Dichloropropane ND<10 <br /> I 3-Dichloropropanc ND<10 <br /> 2 2-Dscliloropropane ND<10 Comments i <br /> 10-Dichloropropene ND<10 Surrogate Recoieries(`%.) <br />' cis-13-Dichloropropene ND<10 Dibromotluoiornethane 106 <br /> trans-13-Dichloropropene ND<10 Toluene-d8 100 <br /> Ethylene dsbromide ND<10 4-Bromotl0orobenzene 89 <br /> nater and vapor samples are reported in ug/L soil and sludge samples m ug/kg is ipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated water samples 1 0 u,-/L N apor samples 05 siglL solid and sludge samples 5 ug/kg, wipes <br /> 0 2ugANipe ND means not detected above the reporting limit NIA means analvie not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water iminiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> I sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,{m)aceuc acrd ethenyl ester {n)chlornethene (o)dimethylbenzenes <br /> DH5 Certilication No 1644 //- Edward Hamilton, Lab Director <br /> I <br />