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=December 22, 1995 <br /> Wright Project No. 4123-S <br /> Site Closure Report <br /> Each soil sample collected from within the excavation and associated stockpile were collected by <br /> hand advancing a 6-inch long by 2-inch diameter brass liner into the exposed soils of the bucket of <br /> the backhoe. Both ends of the soil-filled liner were then covered with TeflonTM film and a plastic <br /> cap. Each sample was then labeled, placed inside a ZiplocTM bag, and stored inside a chilled ice <br /> cooler for transport to a state-certified Iaboratory for chemical analysis. Sample identification and <br /> chain-of-custody procedures were utilized to ensure sample integrity and to document sample <br /> possession from the time of collection to its ultimate disposal. The sample labels identify the fob <br /> number, sampler, date and time of collection, and sample number unique to the sample. The <br /> samples were collected and transported according to the California Department of Health Services <br /> and Environmental Protection Agency protocols. All sampling equipment and brass liners were <br /> washed prior to and between sampling events in a trisodium phosphate (TSP) detergent solution, <br /> then rinsed in clean drinking'water and final rinsed in deionized water. <br /> The soil stockpile samples collected by Wright personnel were signed over to BTSI personnel <br /> under chain-of-custody documentation for transport to the laboratory. The excavation soil samples <br /> collected by BTSI personnel were also transported under chain-of-custody documentation by BTSI <br /> personnel. <br /> 6.5 Laboratory Analysis- Soil <br /> The soil samples collected from within the excavation (ESW-1 through ESW-5, and EBS-1) were <br /> analyzed by Priority Environmental Labs (PEL), a state-certified laboratory located in Milpitas, <br /> California. Each soil sample was analyzed for the presence of total petroleum hydrocarbons as <br /> gasoline (TPHG), diesel (TPHD), and motor oil. In addition, each soil sample was analyzed <br /> discretely for the presence of volatile organic compounds (VOC) and five priority metals <br /> (cadmium, chromium, lead, nickel, and zinc). The TPHG, TPHD, and motor oil analyses were <br /> conducted utilizing methods 8015/5030 and 8015/3550 with a silica gel clean up. The VOC <br /> analyses was conducted utilizing method 8240 and the metals were analyzed by method 7130, <br /> 7190, 7420, 7520, and 7950. Tables 3A and 3B present a summary of the analytical results of the <br /> soil samples collected from within the excavation. A copy of the laboratory report and associated <br /> chain-of-custody documentation for these soil samples is included in Appendix B. <br /> The soil stockpile samples were composited by PEL into two samples, designated as Composite <br /> Sample A and Composite Sample B. Composite Sample A consists of soil stockpile samples <br /> COTSP-1, COTSP-3, COTSP-5, and COTSP-7. Composite Sample B consists of soil stockpile <br /> samples COTSP-2, COTSP-4, COTSP-6,and COTSP-8. Composite Sample A was analyzed for <br /> the presence of TPHG; TPHD; motor oil; benzene, toluene, ethyl benzene, and total xylenes <br /> (BTEX); total recoverable petroleum hydrocarbons (TRPH), halogenated volatile organic <br /> compounds (HVOC), semi-volatile organic compounds (SVOC), and five priority metals <br /> (cadmium, chromium, lead, nickel,and zinc). Composite Sample B was analyzed for the presence <br /> of TPHD, motor oil, and TRPH. PEL utilized methods 8015/5030 and 8015/3510 for the TPHG, <br /> TPHD, and motor oil analyses. Method 8020 was utilized-for the BTEX analyses and method_ <br />- 418.1 was utilized for the TRPH analysis. The HVOC analyses was conducted utilizing method <br /> 8010 and the SVOC analyses was conducted utilizing method 8270. The metal analyses were <br /> conducted utilizing methods 7130, 7190, 7420, 7520, and 7950. The analyses requested for the <br /> stockpile composite samples were consistent with the requirements established by Altamont <br /> Landfill, a Class II landfill located in Livermore, California. PEL utilized methods approved by <br /> the Central Valley Water Quality Control Board and the Environmental Protection Agency. Tables <br /> 4A and 4B present a summary of the analytical results of the soil stockpile samples. A copy of the <br /> laboratory report and associated chain-of-custody documentation for these soil samples is included <br /> in Appendix B. <br /> 6 <br />