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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> I 4 MICA PBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> h2n//www mccampbell com E-mail main@mccampbell conn
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<br /> Advanced GeoEnvironmental Client Project ID D 1 K Tracy Date Sampled 11/28/01
<br /> 837 Shaw Road Enterprises Date Received 11/30/01
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<br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/04-12/07/01
<br /> Chent P O Date Analyzed 12104-12/07/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 84528
<br /> Client ID P-15120to25
<br /> Matrix W
<br /> Rcp=ng L:m t Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone c6) ND<l5 50 25 trans-1,3-Dichloropropene ND 10 50
<br /> Benzene 3 8 10 5 0 Ethylene dibromide ND 1 0 50
<br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 5 0
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichlaromethane ND 1 0 5 0 lodomethane ND 1 0 50
<br /> Bromoform ND 10 5 0 lsopropylbenzene ND 1 0 50
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 so
<br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND l 0 50
<br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride" ND<2 0 1 0 5 0
<br /> cert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone`s ND 1 0 50
<br /> Carbon Temchlonde P ND 10 5 0 Methyl Cert-Butyl Ether(MTBE) 1 0 5 0
<br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 25
<br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 50
<br /> 2-Chloroethyl Vinyl Ethe ° ND 10 5 0 StyreneIkIND 1 0 5 0
<br /> Chloroform ND 1 0 5 0 1 1,1,2-Tetrachloroethane ND 10 5 0
<br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 1 0 50
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethane ND<2 0 1 0 50
<br /> 4-Chlorotoluene ND 10 5 0 Toluene 2 8 1 0 5 0
<br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 12-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromornethane ND 1 0 5 0 1,1,1-Tnchloroethane ND l 0 5 0
<br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND 10 5 0 Tnchloroethene ND 1 0 50
<br /> 1 4-Dichlorobenzene ND 10 5 0 Tnchlorofluoromethane ND 1 0 5 0
<br /> DlchlorodifluoT'Oniethane ND 10 5 0 1,2,3-Tnehloropropane ND 1 0 50
<br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 1 0 50
<br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0
<br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate') - ND 5 0 25
<br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride n ND 1 0 5 0
<br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xyienes total 23 1 10 5 0
<br /> 1,2-Dichloropropane ND 10 5 0 Comments i
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane 108
<br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 100
<br /> cis-1,3-Dichloropropene ND 10 5 0 4-Bromotluorobenzene 100
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting hrrnt N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2-
<br /> i pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 Vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Harrulton,Lab Director
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