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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCANDBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampliell co m E-mail matn@mccampbell com <br /> Advanced GeoBnvironmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 11/30-12112101 <br /> Client P O Date Analyzed 11/30-12/12/01 <br /> Gasoline Range (C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602 California RWQCB(SF Bay Region)method GCF1D(5030) <br /> Lab ID Client 1D Matnx TPH(g)+ MTBE Benzene Toluene Ethyl Xylenes %Recovery <br /> benzene Surrogate <br /> 84503 20)16(1901 W 1100,a ND 190 16 14 26 --- <br /> 84504 P16(36- W ND ND ND ND ND ND 104 <br /> 40)/112901 <br /> 84505 P 16(96- W ND ND ND ND ND ND 106 <br /> 100)/112901 <br /> 84506 P16(76- W ND ND ND ND ND ND 107 <br /> 80)/112901 <br /> 84507 P16(114- W 54,a ND 1 6 059 ND 1 0 106 <br /> 118)/112901 <br /> 84508 P17(18 W 740,a 70 35 17 30 120 102 <br /> 22)/112901 <br /> 84509 P 17(42- W 260,a ND 13 1 3 25 12 107 <br /> 46)/112901 <br /> 84510 80)/1 12901 W 740,a ND 16 11 20 86 --- <br />' Reporting Limit unless W 50 ug/L 5 0 0 5 0 5 0 5 - 05 <br /> otherwise stated,ND <br /> means not detected above <br /> the reporting limit S 1 0 mglkg 0 05 0 005 0 005 0 005 0 005 <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br />' #cluttered chromatogram,sample peak coelutes with surrogate peak <br /> `The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analyttcal is not responsible for their <br />' interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br /> gasoline';), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant,biologically altered gasoline),e)TPH pattern that does not appear to be derived from gasoline(9),t) <br /> one to a few isolated peaks present, g)strongly aged gasoline or diesel range compounds are significant, h)lighter than water immiscible <br /> sheen is present,i)liquid sample that contains greater than N5 vol %sediment,l)no recognizable pattern <br /> DHS Certificatton No 1644 Edward Hamilton,Lab Director <br />