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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httD//www mccampbell com E-mail main@rnccampbell coat <br /> 16 <br />' Advanced GeoEnvtronrnental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br />' 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> [Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84508 <br /> Client ID P17(18-22)/112901 <br /> Matrix W <br /> * Reporting Limit Repamng Limit <br /> Compound Concentration W S Compound Concentration* W S <br /> Acetone @ ND<50 50 25 trans-1 3-Dichloropropene ND<5 0 l 0 5 0 <br /> Benzene 28 1 0 5 0 Ethylene dibromide ND<50 10 50 <br /> Bromobenzene ND<5 0 10 50 1 Ethylbenzene 24 1 0 5 0 <br /> Bromochloromethane ND<5 0 1 10 50 Hexachlorobutadiene ND<25 50 25 <br /> Dromodicnloromethane ND<5 0 10 5 0 lodomethane ND<5 0 1 0 5 0 <br /> Bromotonn ND<5 0 1 0 5 0 Isopropylbenzene ND<5 0 l D 5 0 I <br />' Bromomethane ND<5 0 1 0 50 p4sopropy€toluene ND<5 0 1 10 X 5 0 <br /> n-Butyl benzene ND<5 0 10 50 Methyl butyl ketone ND<5 0 1 0 _'0 <br /> sec-Butyl benzene ND<5 0 1 0 50 Methylene Chlonde` ND<10 1 0 50 <br /> tert-Butyl benzene ND<5 0 10 50 Methyl ethyl ketone i ND<10 20 10 <br /> Carbon Disulfide ND<5 0 1 0 50 Methyl isobutyl ketones' ND<5 0 10 50 <br /> Carbon Tetrachloride ND<5 0 1 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlorobenzene ND<5 0 1 0 50 Naphthalene ND<25 50 25 <br /> Chloroethane ND<5 0 l 0 50 n-Propy€benzene 55 1 0 50 <br />' 2-Chloroethyl Vinyl Ether() ND<5 0 1 0 5 0 Styrene ND<5 0 1 0 5 0 <br /> Chloroform ND<5 0 r 1 0 r 5 0 1,1 1,2-Tetrachloroethane ND<5 0 1 0 5 0 <br /> Chloromethane ND<5 0 1 0 50 1,1,2,2-Tetrachloroethane ND<50 1 0 50 <br /> 2-Chlorotoluene ND<5 0 10 5 0 Tetrachloroethene ND<5 0 1 0 50 <br />' 4-Chlorotoluene ND<5 0 1 0 5 0 TolueneM 14 1 0 50 <br /> Dibromoehloromethane Nl><5 0 1 0 50 1,2,3-Tnchlorobenzenc ND<25 50 25 <br /> 1,2-Dibromo-3-chloropropane ND<10 2 0 10 1 2,4-Tnchlorobenzene ND<25 50 25 <br /> Dibromomethane ND<5 0 1 0 5 0 1 l,l-Trichloroethane ND<5 0 _10_J 5 0 <br />' <br /> 12-Dichlorobenzene ND<5 0 10 5 0 1,1,2-Tnchloroethane ND<5 0 1 0 5 0 <br /> 1,3-Dichlorobenzene ND<5 0 10 50 Trichloroethene ND<5 0 1 0 5 0 <br /> 1,4-Dichlorobenzene ND<5 0 1 0 5 0 Trichlorofluoromethane ND<5 0 1 0 50 <br /> Dichlorodifluoromethane ND<5 0 l 0 50 1,2,3-Trichloropropane ND<5 0 10 50 <br /> 1,1-Dichloroethane ND<5 0 1 0 5 0 1,2,4-Tnmethylbenzene 45 1 0 50 <br /> 1,2-Dichloroedme ND<5 0 10 50 1,3,5-Tnmethylben2ene 1 10 1 0 50 <br /> 1,1-Dichloroethene ND<5 0 1 0 5 0 Vinyl Acetate ND<25 5 0 25 <br /> cis-1,2-Dichloroethene ND<5 0 1 0 5 0 Vinyl Chloride cm ND<5 0 1 0 5 0 <br />' trans-1,2-Dichloroethene ND<5 0 1 0 5 0 Xylenes,total 95 1 0 5 0 <br /> 1,2-Dichloropropane ND<5 0 1 0 5 0 Comments <br /> 1 3-Dichloropropane ND<5 0 1 0 50 Surrogate Recoveries(%} <br /> 2,2-Dichleropropanc ND<5 0 1 0 50 Dibromotluoromethane 101 <br />' <br /> IJ-Dichloropropene ND<5 0 1 0 50 Toluene-d8 97 <br /> cis-1,3-Dichloropropene ND<5 D 1 0 50 4-Bromotluorobenzene 94 <br /> water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 voi % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />