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I <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httn//www mecampbelf cnm E-mail main@mccampbell com <br />' Advanced GeoEnviromnentai Client Project ID D I K Trac Ent Date Sampled 11/29/01 <br /> 3 Y <br />' 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Chent Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> [Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 84510 <br /> Client ID P17(76-80)/112901 <br /> Matrix W <br /> Reporting LimitRepornng Limn <br /> Compound Concentration* W S Compound Concentration' W S <br /> Acetone ibl ND<1� 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene 11 10 5 0 Ethylene dibromide ND 1 0 5 0 <br /> Bromobe izene ND 1 0 5 0 Ethylbenzene 12 ] 0 5 0 <br /> Bromochlotomethane ND 10 5 0 Hexac,hlorobutadiene ND 5 0 25 <br /> Bromodichioromethane ND 1 0 5 0 lodomethane ND 3 0 5 0 <br /> Bromotorm ND 1 0 5 0 Isopropylbenzene 1 8 1 0 5 0 <br /> I Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene 3 4 10 5 0 i Methyl butyl ketone ND —10 5 0 <br /> sea-Butyl benzene l 0 10 5 0 Methylene Chloride`` i ND<2 0 1 0 5 0 <br /> tent-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isoburyl ketones ND 1 0 5 0 <br /> lie Carbon Tetrachloride ND to 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorebenzene ND 10 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene 6 0 1 0 50 <br /> _-Chloroethyl Vinyl Ether" ND 10 5 0 Styrene i ND 1 0 5 0 <br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND l 0 5 0 1 1,2 2-Tetrachloroethane ND 1 0 5 0 <br /> 2 Chiorotoiuene ND 1 0 5 0 Tetrachloroethene ND l 0 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene tit 62 1 0 5 0 <br /> Dioromochloromethane ND 10 5 0 1 2 3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlombenzene ND 5 0 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Trichloroethane ND 1 0 5 0 <br /> 1 2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 1 0 5 0 <br /> 1 3-Dichlorobenzene ND 10 5 0 Tnchloroethene ND 1 0 5 0 <br /> 1,4-Dtchlorobenzene ND 1 0 5 0 Tnehlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2 3-Tnchloropropane ND 1 0 5 0 <br />' 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene 37 1 0 5 0 <br /> 1 2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0 <br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate " ND 5 0 25 <br /> I cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 707: 5 0 <br /> trans-l,2-Dichloroethene ND 10 0 Xylenes,total 43 1 0 5 0 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND l 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND T__0_ 5 0 Dibromofluoromethane 105 <br /> 1,1-Dichloropropene ND 1 0 5 0 TolueneA8 95 <br /> LIS-1,3-Dichloropropene ND 1 0 5 0 4-Bromotluorobenzene 1 1 1 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporung limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 voi % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />