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1 <br /> I 10 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' MCCATNIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> • 24 http//wwwrnccampbelIco E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/30/01 <br />' 837 Shaw Road Date Received 12/04/01 <br /> Stockton,CA 95215 Client Contact Tun.Cuellar Date Extracted 12/07-12/11/01 <br /> tClient P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84751 <br /> Client ID P18(114-118)/113001 <br /> Matrix W <br />' Reporting Limit Repormig Ltmu <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone tni ND<10 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 1 0 5 0 <br />' Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 10 50 Hexachlorohutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 1 0 50 <br />' Bromomethane ND 1 0 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde° ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 l0 <br /> l <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketones ND 10 50 <br /> ie Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 5 0 <br />' 2-Chloroethyl Vinyl Ether` ND 1 0 50 Styrene ND l i7 5 0 <br /> 0 <br /> Chlorotorm ND 1 050 1,1,1,2-'Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 1 0 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnehlorobenzene ND 50 25 <br /> Dibromornethane ND 1 0 50 1,1,1-Tnehloroethane ND 1 0 _)0 <br /> 1,2-Dichlorobenzene ND 10 50 1 1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 'Fnchlorofluoromethane ND 1 0 50 <br /> Dichlarodrfluoromethane ND 1 0 50 1,2,3-Trichloropropane ND 1 0 50 <br /> 1,1-Dichloroethane ND 1 0 50 1,2 4-Tnmethylbenzene ND 1 05 0 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroetheze ND 1 0 50 Vinyl Acetate m ND 5 0 25 <br /> t.3s-1,2-Dtchloroethene ND 1 0 50 Vinyl Chloride " ND 1 0 50 <br /> trans-l,2-Dichloroethene ND 1 0 50 Xylenes,total ND 1 0 H 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 103 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 1 0 1 50 4-Bromolluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts m ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1) liquid sample that contains greater than --5 vol % <br /> I sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (D) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS-Certification No 1644 Edward Harmlton, Lab Director <br />