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110 2nd Avenge South,#D7,Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 1 http//www mccampbelI co m E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> Chent P O Date Analyzed 12/04-12/07/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 84503 84504 84505 84506 <br /> F 16(15- P16(36- P 16(96- P 16(76- Reporting Limit <br /> Client ID 20}/I 12901 40)/112901 100)1112901 80)/112901 <br /> Matrix W W W W 5 W <br /> Compound Concentration* ug/kg ug/L <br /> LDi-isopropyl Ether(DIPS) ND ND ND ND 50 10 <br /> Ethyl tent-Butyl Ether(ETRE) ND ND ND ND 50 10 <br /> I <br /> Methyl tert-Butyl Ether(MT$$) 1 1 34 ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 10 <br /> tert-Butanol ND ND ND ND 25 50 <br /> Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> ------------ <br /> Surrogate Recoveries(%} <br />' Dibromofluoromethane 100 108 107 108 " <br />' Comments <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(1)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />