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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mcc_aLnUbell_com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed 12103-12/06/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> BPA method 8260 modified <br /> Lab ID 84515 84516 84517 84518 <br /> 1 Reporting Limit <br /> Client ID CPT13(136- CPT14(21- CPT14(39- CPT14(62- <br /> 140)/112601 25)112701 43)112701 67)112701 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND ND ND ND 50 1 0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> tert-Butanol ND ND ND ND 25 50 <br /> Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibrornofluoromethane 107 107 107 105 <br />' Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br />' high organic content <br /> DHS Certification No 1644 Edward HannIton,Lab Director <br />