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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mEeampbell com E-mail mamCmccampbell com <br /> iAdvanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27101 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12103-12/06/01 <br /> Client P Ct Date Analyzed 12/03-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84517 <br /> Client ID CPT14(39-43)/112701 <br /> Matrix W <br /> Reporting Limt Reporting Limit <br /> Compound Concentration* W S Compound Concentration* W I S <br /> Acetone ND<15 50 25 trans-1,3 Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND to 5 0 1 Ethylbenzene ND 10 5 0 <br /> Bromochiornmethane ND 10 50 Hexachlorobutadiene ND 50 3 25 <br /> Bromodichioromethane ND l 0 5 0 lodomethane ND 10 5 0 <br /> Bromotorm ND 1 0 50 Isopropylben7ene ND 1 0 5 0 <br /> Bromomethane ND 10 5 0 p-lsopronvi toluene ND l 0 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ' ND 1 0 5 0 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride" ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 1 0 50 Methvl isobutvi ketone'91 ND 1 0 5 0 <br /> Carbon Tetrachloride ND to L_5O_ Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND -50 25 <br /> Chloroethane ND 1 0 50 n-Propvl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Ether` ND t 0 5 0 Styrene" ND 10 50 <br /> Chloroform ND L 0 1 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 1 0 1 5 0 1 1,2 2-Tetrachloroethane ND lo 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachioromthene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene{ ND 1 0 5 0 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> T 2-Dibromo-3-chioropropane ND 2 0 10 1,2 4-Trichlorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dtchlorobenzene AFD 1 0 50 1,1,2-Tnchloroethane ND 1 0 5 0 <br /> 1,3-DiOlorobenzene ND 10 5 0 Trichloroethene ND 1 0 5 0 <br /> 1,4-1)tchiorobenzene ND 10 50 Trichlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2 3-Tnchloropropane ND 1 0 5 0 <br /> 1 1-Dichioroethane ND 1 0 50 1,2,4-TnrnethyiWzene ND 1 0 5 0 <br /> 1,2-Dtchloroethane ND 1 0 50 1,3,5-Trtmethylbenzene ND 1 0 5 0 <br /> 1 1-Dichloroethene ND 1 0 50 Vinyl Acetate '°' - ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride i'I ND 1 0 5 0 <br /> trans-t,2-Dichloroethene ND l 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1 2-Dichloropropane ND I O 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 115 <br /> 1,I-Dichloropropene ND 1 0 50 Toluene-d8 115 <br /> OS-1,3-Dichloropropene ND 1 0 50 4-Bromofluorobenzent. 96 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroothoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, (7) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (in) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />