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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http/lwww mccampbell com E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 06/13/01 <br /> 837 Shaw Road Date Received 06/14/01 <br /> Stockton,CA 95215 Client Contact Tun Cuellar Date Extracted 06/14-06/15/01 <br /> Client P O Date Analyzed 06/14-06/15101 <br />' Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> LabrD 69745 69746 69747 69748 <br /> MW1/06130 MW2/06130 MW3/06130 MW4/06130 Reporting Limit <br /> Client ID 1 l 1 1 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND<2 5 ND<2 5 ND<5 0 ND<2 5 so 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<2 5 ND<2 5 ND<5 0 ND<2 5 50 to <br /> Methyl tert-Butyl Ether(MTBE) 65 52 ND<5 0 60 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<2 5 ND<2 5 ND<5 0 ND<2 5 50 1 0 <br /> tert-Butanol 29 ND<12 5 ND<25 ND<12 5 25 50 <br /> IMethanol ND<1250 ND<1250 ND<2500 ND<1250 2500 500 <br /> Ethanol ND<125 ND<125 ND<250 ND<125 250 50 <br /> Surrogate Recoveries(%) <br />' Dibromotluoromethane 98 98 95 100 <br />' Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A rneans surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 �( Edward Hamilton, Lab Director <br />