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110 2nd Avenue South #D7 Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Teiephone 925-798 1620 Fax 925-798-1622 <br /> 7ho ht /Iwww inecarripbell cam E-mail niainrnccarnpbrll coni <br /> Advanced GeoEnvlronmental, Inc Client Project ID Threee B's Date Sampled 09/17/03 <br /> 837 Shaw Road Date Received 09/18/03 - <br />' Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 09/24/03 <br /> Client P Q Date Analyzed 09/24/03 <br />' Oxygenated Volatile Organics +EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309344 <br />' Lab ID 0309344-OOIC 0309344-002C 0309344-003C 10309344-004C <br /> Client ID MW1 MW1IA MWl lB MW11C Reporting Limit for <br /> I <br />' Matrix — W _- - - W W W DF=1 I <br /> DF 3 3 1 1 1 5 W <br />' Compound Concentration ug/kg Ag/I, <br /> Diisopropyl ether(DIPS) ND<1 7 ND ND ND NA 05 <br />' Ethyl tert-butyl ether(ETBE) ND<l 7 ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 12 75 067 1 3 NA 05 <br /> tent-Amyl methyl ether(TAME) ND<1 7 ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) 19 24 ND ND NA 50 <br /> 1,2-Dibromoethane(EBS) ND<1 7 ND ND ND NA 05 <br /> 1 1,2-Dichloroethane(1,2-DCA) ND<l 7 46 ND ND NA 05 <br />' Surrogate Recoveries(%) <br /> %SS 102 107 112 109 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in lig/kg, wipe samples to Ag/wipe, <br /> product/oiUnon-aqueous liquid samples in mg/L _ <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> 1 <br /> I <br /> DHS Certification No 1644 '} Angela Rydehus, Lab Manager <br />