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110 2nd Avenue South #D7,Pacheco,CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-798 1620 Fax 925-798-1622 <br /> h //www mrcampbell com E-mail main@rricrarripbell cum <br /> Advanced GeoEnvironmental, Inc Chent Project ID 3 B's Truck Plaza Date Sampled 06/25/03 <br />' 837 Shaw Road Date Received 06/26/03 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 06/30/03-07/02103 <br /> CIient P O Date Analyzed 06/30/03.07/02103 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW9260B Work Order 0306567 <br /> Lab ID 0306567-013B 0306567-014B 0306567-015B 0306567-016B <br /> Client ID MW8D MW8E MW8F MW9D <br /> Reporting Limit for <br /> Matrix WW W W DF—1 <br /> DF 1 — 1 -----I—---i-- — — --I- <br /> 1— 5 W <br /> I <br />' Compound Concentration ug/kg pg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> Benzene 3 8 19 5 4 ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> Dnsopropyl ether(DIPE) ND ND ND ND NA 0 5 <br /> Ethylbenzene ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(E7 BE) ND ND ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 0 5 <br /> Toluene ND ND ND ND NA 05 <br /> IXylenes ND ND ND ND NA 0-5 <br /> Surrogate Recoveries(%) <br /> %SSI 113 113F96 <br /> 115 <br /> 7 <br /> %S52 95 9 94 9 962 <br /> %SS3 102 101 102 102 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soiVsludge/solid samples in lig/kg, wipe samples inµg/wipe, <br /> product/od/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,l)sample diluted due to high <br /> f ]organic content <br /> I <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />