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110 2nd Avenue South,t107 Pacheco CA 94553 5560 <br /> 4 McCampbell Analytical, Inc. Telephone 925-798-1620 rax 925 798-1622 <br /> Website www mccampbell con= L-mail roam@mcearnpbell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID Three B's Date Sampled 09/15/04 <br /> 837 Shaw Road Date Received 09/16/04 <br /> Client Contact Tim Cuellar Date Extracted 09/18/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analysed 09/18/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method 5W8260B Work Oidcr 0409233 <br />' Lab ID 0409233-005C 0409233-006C 10409233-007C , 0409233-008C — <br /> Client ID MW9E/9/15/04 MW12A/9/15/04 MW12B/9/15104,MW12C/9/15104 Reporting Limit for <br /> Matrix W W W W DP—1 <br /> DF 1 1 1 i ] S W <br /> Compound Concentration I ug/kg pg/L <br /> tell-Amyl methyl ether(TAME) ND ND�— ND — j ND NA 05 <br /> t-Butyl alcohol(TBA) ND ND I ND i ND NA 50 <br /> 1,2-Dlbromoethane(EDB) ND --ND ND — ND NA 0 5 <br /> 1,2-Dichloroethane(1 2-DCA) ND ND ND ND NA 05 <br /> Diisopropyl ether(DIPS) ND ND ND ND NA 05 <br />' Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> Surrogate Recoveries <br /> %SS 112 111 113 113 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported to pg/L soil/sludge/solid samples in pg/kg, wipe samples to pglwlpe, <br /> product/oil/non-aqueous liquid samples in mg1L <br /> ND means not detCULd above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br />