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STT Submission 2005-05-0124 <br /> Gas/BTEX Fuel Oxygenates by 8260B <br /> SECOR-Sacramento <br /> Attn Clint Harms <br /> 3017 Kilgore Road, Suite 100 <br /> Rancho Cordova, CA 95670 <br /> Phone (916)861-0400 Fax (916)861-0430 <br /> Project 77CP 68671 03 0003 Received 05/03/2005 16 10 <br /> Conoco Philips Site#8671 <br /> Site 8606 Thornton Road, Stockton, CA <br /> Batch QC Report <br /> Prep(s) 503013 Test(s) 8260E <br /> Matrix Spike( MS 1 MSD ) Soil QC Batch #2005105107-3B 69 <br /> MS/MSD Lab ID 2005-04-0856-001 <br /> M5 2005105107-313 69-039 Extracted 05/07/2005 Analyzed 05/07/2005 21 39 <br /> Dilution 1 00 <br /> MSD 2005105107-38 69-058 Extracted 05/07/2005 Analyzed 05/07/2005 21 58 <br /> Dilution1 00 <br /> Compound Conc m IKg Spk Level Recove % Limits% Flags <br /> MS MSD Sample rnq1Kq MS MSD RPD Rec RPD MS MSD <br /> Methyl tert-butyl ether 00406 00427 ND 0046904 866 879 1 5 65-165 20 <br /> Benzene 00455 00464 ND 0046904 970 954 17 69-129 20 <br /> Toluene 00436 00500 ND 0046904 930 1029 101 70-130 20 <br /> Surrogate(s) <br /> 1,2-Dichloroethane-d4 466 477 500 932 953 72-124 <br /> Toluene-d8 506 1562 500 1012 1124 75-116 <br /> Severn Trent Laboratories, Inc 05/181200512 14 <br /> STL San Francisco*1220 Quarry Lane Pleasanton,CA 94566 <br /> A part of 60ve Tient Plc Tel 925 484 1919 Fax 925 484 1096*www stl-inc com*CA DHS ELAP#2496 Page 7 of 8 <br />