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QC Sample Results Client: Stantec Consulting Corp. TestAmerica Job ID:440-84744-1 Project/Site: CVX 9-6171, Stockton Method: 8260B/5030B -Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID:440-84744-1 MSD Client Sample ID: BA-1@ 10 Matrix:Solid Prep Type:Total/NA Analysis Batch: 198077 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,2-Dibromo-3-Chloropropane ND 0.0500 0.0437 mg/Kg 87 4 0-150 0 30 1,2-Dibromoethane(EDB) ND 0.0500 0.0564 mg/Kg 113 65-140 1 25 1,2-Dichlorobenzene ND 0.0500 0.0547 mg/Kg 109 70-130 0 25 1,2-Dichloroethane ND 0.0500 0.0588 mg/Kg 118 60-150 1 25 1,2-Dichloropropane ND 0.0500 0.0561 mg/Kg 112 65-130 0 20 1,3,5-Trimethylbenzene ND 0.0500 0.0520 mg/Kg 104 65-135 3 25 El 1,3-Dichlorobenzene ND 0.0500 0.0524 mg/Kg 105 70-130 1 25 1,3-Dichloropropane ND 0.0500 0.0557 mg/Kg 111 65-140 3 25 1,4-Dichlorobenzene ND 0.0500 0.0532 mg/Kg 106 70-130 0 25 2,2-Dichloropropane ND 0.0500 0.0524 mg/Kg 105 65-150 0 25 2-Chlorotoluene ND 0.0500 0.0499 mg/Kg 100 60-135 3 25 4-Chlorotoluene ND 0.0500 0.0532 mg/Kg 106 65-135 2 25 Benzene ND 0.0500 0.0511 mg/Kg 102 65-130 3 20 Bromobenzene ND 0.0500 0.0553 mg/Kg 111 65-140 1 25 Bromochloromethane ND 0.0500 0.0602 mg/Kg 120 65-145 0 25 Bromodichloromethane ND 0.0500 0.0610 mg/Kg 122 65-145 1 20 Bromoform ND 0.0500 0.0540 mg/Kg 108 50-145 2 30 Bromomethane ND 0.0500 0.0580 mg/Kg 116 60-155 1 25 Carbon tetrachloride ND 0.0500 0.0520 mg/Kg 104 60-145 1 25 Chlorobenzene ND 0.0500 0.0508 mg/Kg 102 70-130 3 25 Chloroethane ND 0.0500 0.0567 mg/Kg 113 60-150 4 25 Chloroform ND 0.0500 0.0580 mg/Kg 116 65-135 2 20 Chloromethane ND 0.0500 0.0511 mg/Kg 102 40-145 4 25 cis-1,2-Dichloroethene ND 0.0500 0.0595 mg/Kg 119 65-135 1 25 i cis-1,3-Dichloropropene ND 0.0500 0.0600 mg/Kg 120 70-135 2 25 Dibromochloromethane ND 0.0500 0.0579 mg/Kg 116 60-145 3 25 Dibromomethane ND 0.0500 0.0596 mg/Kg 119 65-140 0 25 Dichlorodifluoromethane ND 0.0500 0.0466 mg/Kg 93 30-160 7 35 Ethanol ND 0.500 0.523 mg/Kg 105 30-165 13 40 Ethylbenzene ND 0.0500 0.0498 mg/Kg 100 70-135 5 25 Ethyl-t-butyl ether(ETBE) ND 0.0500 0.0557 mg/Kg 111 60-145 0 30 Hexachlorobutadiene ND 0.0500 0.0495 mg/Kg 99 50-145 3 35 Isopropyl Ether(DIPE) ND 0.0500 0.0544 mg/Kg 109 60-150 1 25 Isopropyl benzene ND 0.0500 0.0488 mg/Kg 98 70-145 4 25 m,p-Xylene ND 0.100 0.0983 mg/Kg 98 70-130 6 25 Methylene Chloride ND 0.0500 0.0638 mg/Kg 128 55-145 2 25 Methyl-t-Butyl Ether(MTBE) ND 0.0500 0.0580 mg/Kg 116 55-155 1 35 Naphthalene ND 0.0500 0.0489 mg/Kg 98 40-150 2 40 n-Butylbenzene ND 0.0500 0.0504 mg/Kg 101 55-145 3 30 N-Propylbenzene ND 0.0500 0.0506 mg/Kg 101 65-140 4 25 o-Xylene ND 0.0500 0.0526 mg/Kg 105 65-130 4 25 p-Isopropyltoluene ND 0.0500 0.0519 mg/Kg 104 60-140 2 25 sec-Butylbenzene ND 0.0500 0.0518 mg/Kg 104 60-135 2 25 Styrene ND 0.0500 0.0550 mg/Kg 110 70-140 2 25 Tert-amyl-methyl ether(TAME) ND 0.0500 0.0572 mg/Kg 114 60-150 3 25 tert-Butyl alcohol(TBA) ND 0.250 0.253 mg/Kg 101 65-145 14 30 tert-Butylbenzene ND 0.0500 0.0487 mg/Kg 97 60-140 5 25 Tetrachloroethene ND 0.0500 0.0501 mg/Kg 100 65-135 6 25 TestAmerica Irvine Page 21 of 29 8/7/2014