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Case Narrative <br /> Client:Stantec Consulting Corp. TestAmerica Job ID:440-84727-1 <br /> Project/Site:CVX 9-6171,Stockton <br /> Job ID: 440-84727-1 <br /> Laboratory:TestAmerica Irvine <br /> Narrative <br /> Job Narrative <br /> 440-84727-1 <br /> Comments <br /> No additional comments. <br /> Receipt <br /> The samples were received on 8/5/2014 10:30 AM;the samples arrived in good condition,properly preserved and,where required,on ice. <br /> The temperature of the cooler at receipt was 4.1°C. <br /> Except: <br /> The Chain-of-Custody(COC)was incomplete as received and/or improperly completed.No sample date and/or time on COC,logged in <br /> per container labels. <br /> GC/MS VOA <br /> Method(s)82608:The following sample(s)were collected in properly preserved vials for analysis of volatile organic compounds(VOCs). <br /> However,the pH was outside the required criteria when verified by the laboratory,and corrective action was not possible:BA-2-W <br /> (440-84727-2). pH=3 <br /> Method(s)624,82606:Samples were preserved,but had pH=3 due to buffer effect. <br /> No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. <br /> GC VOA <br /> No analytical or quality issues were noted,other than those described in the Definitions/Glossary page. <br /> GC Semi VOA <br /> Method(s)80156:Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate(MS/MSD)associated with <br /> batch 197846. The laboratory control sample(LCS)was performed in duplicate to provide precision data for this batch. <br /> No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. <br /> Organic Prep <br /> No analytical or quality issues were noted,other than those described in the Definitions/Glossary page. <br /> VOA Prep <br /> No analytical or quality issues were noted,other than those described in the Definitions/Glossary page. <br /> TestAmerica Irvine <br /> Page 4 of 26 8/7/2014 <br />