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Quality Control Data <br /> Client:ARCADIS TestAmerica Job ID: 720-33917-1 <br /> Project/Site: UPRR-Tracy Yard <br /> Method: 300.0 -Anions, Ion Chromatography (Continued) <br /> Lab Sample ID: 720-33995-A-3 MSD Client Sample ID: 720-33995-A-3 MSD <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 88033 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Nitrite as N ND 30.4 29.8 mg/L 98 80-120 1 20 <br /> Sulfate 27 100 124 mg/L 97 80-120 1 20 <br /> Chloride 30 100 125 mg/L 95 80-120 0 20 <br /> Method: 350.2 - Nitrogen, Ammonia, Distillation <br /> Lab Sample ID: MB 500-108079/1-A Client Sample ID: MB 500-108079/1-A <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 108279 Prep Batch: 108079 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Ammonia(as N) ND 0.20 mg/L 03/20/1113:16 03/22/11 12:43 1 <br /> Lab Sample ID: LCS 500-108079/2-A Client Sample ID: LCS 500-108079/2-A <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 108279 Prep Batch: 108079 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Ammonia(as N) 2.50 2.39 mg/L 96 80-120 <br /> Lab Sample ID: 500-31894-B-1-B MS Client Sample ID: 500-31894-B-1-B MS <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 108279 Prep Batch: 108079 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Ammonia(as N) 0.23 2.50 2.63 mg/L 96 75-125 <br /> Lab Sample ID: 500-31894-B-1-C MSD Client Sample ID: 500-31894-B-1-C MSD <br /> Matrix:Water Prep Type: Total/NA <br /> Analysis Batch: 108279 Prep Batch: 108079 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Ammonia(as N) 0.23 2.50 2.59 mg/L 94 75-125 1 20 <br /> Method: 376.1 -Sulfide <br /> Lab Sample ID: MB 500-108332/1 Client Sample ID: MB 500-108332/1 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 108332 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Sulfide ND 1.0 mg/L 03/22/1122:15 1 <br /> Lab Sample ID: LCS 500-108332/2 Client Sample ID: LCS 500-108332/2 <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 108332 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Sulfide 3.86 4.00 mg/L 104 80-120 <br /> TestAmerica San Francisco <br /> Page 19 of 52 04/04/2011 <br />