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Laboratories Inc. _ <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/28/2016 17:22 <br /> 3590 Iron Court Project: Diamond Pet Foods-COELT <br /> Shasta Lake City,CA 96019 Project Number: 010107.08 Task 4 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> BCL Sample ID: 1628545-05 Client Sample Name: Diamond Pet,OB-7, 10/11/2016 1:14:OOPM, David Kirk <br /> MB Lab <br /> Constituent Result Units PQL MDL Method Bias Quals Run# <br /> Dissolved Calcium 84 mg/L 0.10 0.016 EPA-200.7 0.019 1 <br /> Dissolved Magnesium 23 mg/L 0.050 0.019 EPA-200.7 ND 1 <br /> Dissolved Sodium 150 mg/L 0.50 0.051 EPA-200.7 ND 1 <br /> Dissolved Potassium 3.5 mg/L 1.0 0.10 EPA-200.7 ND <br /> Bicarbonate 360 mg/L 10 10 EPA-310.1 ND 2 <br /> Carbonate ND mg/L 5.0 5.0 EPA-310.1 ND 2 <br /> Alkalinity as CaCO3 290 mg/L 4.1 4.1 Calc ND 3 <br /> Chloride 99 mg/L 0.50 0.092 EPA-300.0 ND 4 <br /> Nitrate as N 3.4 mg/L 0.10 0.022 EPA-300.0 ND 4 <br /> Sulfate 110 mg/L 1.0 0.14 EPA-300.0 ND 4 <br /> Dissolved Hardness as CaCO3 300 mg/L 0.50 0.10 Calc ND 3 <br /> pH 7.87 pH Units 0.05 0.05 EPA-150.1 S05 5 <br /> Electrical Conductivity @ 25 C 1110 umhos/c 1.00 1.00 EPA-120.1 6 <br /> M <br /> Total Dissolved Solids @ 180 C 670 mg/L 33 33 EPA-160.1 ND 7 <br /> Total Nitrogen 3.7 mg/L 0.30 0.10 Calc ND 8 <br /> Total Kjeldahl Nitrogen 0.25 mg/L 0.20 0.088 EPA-351.2 ND 9 <br /> Run QC <br /> Run# Method Prep Date Date/Time Analyst Instrument Dilution Batch ID <br /> 1 EPA-200.7 10/14/16 10/19/16 18:17 JRG PE-OP2 1 BZJ1605 <br /> 2 EPA-310.1 10/13/16 10/13/16 17:35 RML MET-1 2 BZJ1199 <br /> 3 Calc 10/12/16 10/28/16 12:41 MSA Calc 1 BZJ1009 <br /> 4 EPA-300.0 10/12/16 10/12/16 16:19 EMW IC1 1 BZJ1056 <br /> 5 EPA-150.1 10/13/16 10/13/16 17:35 RML META 1 BZJ1199 <br /> 6 EPA-120.1 10/13/16 10/13/16 17:35 RML META 1 BZJ1199 <br /> 7 EPA-160.1 10/17/16 10/17/16 14:00 CAD MANUAL 3.333 BZJ1427 <br /> 8 Calc 10/12/16 10/25/16 22:01 AMM Calc 1 BZJ1009 <br /> 9 EPA-351.2 10/17/16 10/24/16 13:15 JMH SC-1 1 BZJ1517 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party. BC Laboratories,Inc.assumes no responsibility for report alteration,separation,detachment or third party interpretation. <br /> Report ID: 1000538621 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 22 of 59 <br />